Agilent Technologies 1100 Series Manuel utilisateur

Agilent 1100 Series

Handheld Control Module

User’s Guide

Agilent Technologies

Hewlett-Packard-Strasse 8

76337 Waldbronn

Germany

Copyright Agilent

Technologies 2000

Reproduction, adaption,

or translation without

prior written permission

is prohibited, except as

allowed under the

Part No. G1323-90006

Edition 01/00,

Printed in Germany

Warranty

The information

contained in this

document is subject to

change without notice.

Agilent Technologies

makes no warranty of

any kind with regard to

this material,

including, but not

limited to, the implied

warranties or

merchantability and

fitness for a particular

purpose.

Agilent Technologies

shall not be liable for

errors contained herein

or for incidental or

consequential damages

in connection with the

furnishing, performance,

or use of this material.

WARNING

For details of safety,

see Safety Information

on page 142

Warning Symbols Used

In This Book

The apparatus is marked

with this symbol when

the user should refer to

the instruction manual

in order to protect the

apparatus against

damage.

User’s Guide

Agilent 1100 Series Handheld Control Module

This book describes how to operate the Agilent 1100 Series modules and

systems for HPLC using the control module, shown opposite. The control

module provides complete local control and monitoring of a single module or

an entire Agilent 1100 Series system. There is no data evaluation in the

control module. The control module allows you to do a variety of HPLC tasks

including automated sample preparation and injection, isocratic, gradient

and multiple method analyses.

Other Books Available:

Each HPLC module is supplied with a Reference Manual which describes

installation, troubleshooting, repair, parts and theory of operation.

The control module is supplied with the following:

• User’s Guide

• Software Overview Guide

• Performance Verification Manual

• Online Information System

In This Book

Solvent cabinet

Vacuum degasser

Pump

Column compartment

Autosampler

Detector

Control module

In This Book

Part 1 “Using the Agilent 1100 Series Control Module”describes the control

module, its features and its functionality.

Part 2 “Using the Agilent 1100 Series Modules”describes how to use the

individual HPLC modules to run isocratic, gradient and multiple-vial analyses

using a single method or more than one method.

Part 3 “Using the Agilent 1100 Series LC System With Control Module”

describes how to run isocratic, gradient and multiple-vial analyses using a

single method or more than one method.

In This Book

Contents

Part 1 Using the Agilent 1100 Series Control Module

1 The Agilent 1100 Series Control Module

Overview over the Agilent 1100 Series control module 18

Control Module Features 19

Control Module Keys 20

Control Module Software 24

Control Module Versions 31

2 Working with the Control Module

How to use the Agilent 1100 Series control module 33

Installing the Control Module 34

General Functions 35

Troubleshooting 36

Inserting and Removing PC cards 37

Working with Methods 38

Time Programming 43

Automating Analyses 44

Displaying Data Graphically 46

Logbooks 48

Printing Screens 49

Connecting External Devices 51

Firmware 53

Updating Firmware in the Control Module 53

Updating Firmware in the LC Modules 54

Coexecution with Agilent ChemStation 58

Contents

Part 2 Using the Agilent 1100 Series Modules

3 Using the Pump

Operational details for the Agilent 1100 Series pumping systems 63

Turning the Pump On and Off 64

Entering Settings 64

Purging the Pump 64

Purging Procedure 65

Adjusting Compressibility 66

Adjusting Stroke Volume 67

Automatic Shut-down 67

Troubleshooting the Pump 68

Tracking Pump History / Pump EMF Limits 68

Resetting the Pump 69

Resetting the Pump Settings 69

4 Using the Degasser

Operational details for the Agilent 1100 Series vacuum degasser 71

Starting the Degasser 72

Removing Gas Bubbles 72

Changing Solvents 73

5 Using the Autosampler

Operational details for the Agilent 1100 Series autosampler 75

Configuring the Autosampler 76

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