Agilent Technologies Cary Eclipse Manuel utilisateur

Cary Eclipse

Fluorescence

Spectrophotometer

User’s Guide

2 Cary Eclipse Fluorescence Spectrophotometer User’s Guide

Notices

2000 and 2011-2013, 2015, 2016

No part of this manual may be

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means (including electronic storage

and retrieval or translation into a

foreign language) without prior

agreement and written consent from

Agilent Technologies, Inc. as governed

by United States and international

Manual Part Number

8510175800

Edition

Seventh edition, September 2016

Printed in Malaysia

Agilent Technologies Australia [M] Pty

Ltd

679 Springvale Road

Mulgrave, Victoria, 3170, Australia

www.agilent.com

Agilent products must only be used in

the manner described in the Agilent

product user guides. Any other use

may result in damage to the product

or personal injury. Agilent is not

responsible for any damages caused,

in whole or in part, by improper use of

the products, unauthorized alterations,

adjustments or modifications to the

products, failure to comply with

procedures in Agilent product user

guides, or use of the products in

violation of applicable laws, rules or

regulations.

Agilent shall not be liable for errors or

damages on products or performance

due to using non-Agilent genuine

parts.

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subject to being changed, without

notice, in future editions. Further, to

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The hardware and/or software

described in this document are

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Restricted Rights Legend

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performance of a U.S. Government

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Software is delivered and licensed as

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defined in DFAR 252.227-7014 (June

1995), or as a “commercial item” as

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or any equivalent agency regulation or

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greater than Restricted Rights as

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1987). U.S. Government users will

receive no greater than Limited Rights

as defined in FAR 52.227-14 (June

1987) or DFAR 252.227-7015 (b)(2)

(November 1995), as applicable in any

technical data.

Safety Notices

A CAUTION notice denotes a hazard.

It calls attention to an operating

procedure, practice, or the like that, if

not correctly performed or adhered to,

could result in damage to the product

or loss of important data. Do not

proceed beyond a CAUTION notice

until the indicated conditions are fully

understood and met.

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice, or the

like that, if not correctly performed or

adhered to, could result in personal

injury or death. Do not proceed

beyond a WARNING notice until the

indicated conditions are fully

understood and met.

WARNING

CAUTION

Contents

Cary Eclipse Fluorescence Spectrophotometer User’s Guide 3

Contents

1. Safety Practices and Hazards 7

Verifying Safe State 7

Lamp module 8

Ultraviolet radiation 8

Electrical hazards 9

Panels, covers and modules 10

Other precautions 10

Warning and information symbols 11

Color coding 13

CE compliance 13

Electromagnetic compatibility 14

EN55011/CISPR11 14

ICES/NMB-001 15

South Korean Class A EMC declaration 15

2. Introduction 17

Installation requirements 17

Documentation 17

Conventions 18

Specifications 18

Environmental 18

Weights and dimensions 19

Power 19

Contents

4 Cary Eclipse Fluorescence Spectrophotometer User’s Guide

Connections 19

Fuses 20

Nitrogen supply 20

Computer placement 20

3. Installation 21

Single cell holder 22

Aligning 24

Other sample holders 25

Purging 25

Nitrogen 25

Pressure regulator and gauge 25

Supply tubing 25

Gas manifold 26

Flowmeter 26

Installing the software 26

Installing the USB-GPIB-HS Converter 28

Registering the Cary Eclipse software 28

Uninstalling the software 29

Software Status Bulletin 29

4. Maintenance and Spare Parts 31

Cleaning 32

Lamp module 32

Replacing 32

Aligning 35

Fuses 38

Contents

Cary Eclipse Fluorescence Spectrophotometer User’s Guide 5

Replacing 38

Checking 39

Spare Parts 39

5. Troubleshooting 41

Instrument offline 42

Connect button instead of Start 42

Instrument performance testing 43

Contents

6 Cary Eclipse Fluorescence Spectrophotometer User’s Guide

This page is intentionally left blank.

Safety Practices and Hazards

Cary Eclipse Fluorescence Spectrophotometer User’s Guide 7

1. Safety Practices and Hazards

Verifying Safe State 7

Lamp module 8

Ultraviolet radiation 8

Electrical hazards 9

Panels, covers and modules 10

Other precautions 10

Warning and information symbols 11

Color coding 13

CE compliance 13

Electromagnetic compatibility 14

Your Agilent Cary Eclipse instrument and accessories have been

carefully designed so that when used properly you have an accurate,

fast, flexible and safe analytical system.

If the equipment is used in a manner not specified by the

manufacturer, the protection provided by the equipment may be

impaired.

Information on safety practices appears throughout the

documentation (both hard copy and online) provided with your

instrument and accessories. Before using the instrument or

accessories, you must thoroughly read these safety practices.

Observe all relevant safety practices at all times.

Verifying Safe State

The following general safety precautions must be observed during all

phases of operation, maintenance and service of this instrument.

Safety Practices and Hazards

8 Cary Eclipse Fluorescence Spectrophotometer User’s Guide

To ensure continued safety of the instrument after maintenance or

service procedures verify the instrument is returned to a safe state

for the user. This includes running performance checks to verify the

instruments safety systems are functioning correctly. Check the

general condition of the instrument during operation for wear or

signs of corrosion that are likely to inhibit function or safety.

Failure to comply with these precautions or with specific warnings

elsewhere in this manual violates safety standards of design,

manufacture, and intended use of the instrument. Agilent

Technologies assumes no liability for the customer’s failure to

comply with these requirements.

Lamp module

The lamp is enclosed in a self-contained module. This module

contains components operating at high voltages. To avoid electric

shock, NEVER disassemble the module.

When operating, the lamp module emits high intensity visible and

ultraviolet (UV) radiation that can cause serious damage to eyes. To

avoid eye damage, never operate the lamp outside the instrument.

WARNING

Eye and Shock Hazard

High voltage Xe flashlamp operating at 1260 kPa. To avoid electric shock or

eye damage, NEVER disassemble the module or look down the hole.

La lampe Xe haut voltage fonctionne à une pression de 1260 kpa. Pour éviter

tout risque électrique et des problèmes oculaires ne jamais ouvrir le module

ou regarder à l’intérieur.

Ultraviolet radiation

Hazardous ultraviolet (UV) radiation is emitted by the xenon flash

lamp in the instrument. This radiation can cause serious damage to

eyes. Never look directly at the UV source lamp.

Safety Practices and Hazards

Cary Eclipse Fluorescence Spectrophotometer User’s Guide 9

Electrical hazards

The Cary Eclipse system and some accessories contain electrical

circuits, devices, and components operating at dangerous voltages.

Contact with these circuits, devices and components can cause death,

serious injury, or painful electrical shock.

Panels or covers which are retained by screws on the

spectrophotometer and accessories and carry a warning may be

opened ONLY by Agilent-trained, Agilent-qualified, or Agilent-

approved customer service representatives. Consult the manuals or

product labels supplied with your computer, monitor and printer to

determine which parts are operator-accessible.

Good grounding is essential to avoid a potentially serious electric

shock hazard. Ensure that there is an integral ground connection

between the metal base of the spectrophotometer and accessories

and the three pin earth-grounded receptacle. Consult the manuals or

product labels supplied with your computer, monitor and printer for

their grounding requirements.

NOTE The safety classification is given as Equipment Class I.

Application of the wrong supply voltage can create a fire hazard and

a potentially serious shock hazard, and could seriously damage the

Cary Eclipse system, accessories and any attached ancillary

equipment.

Do not connect the Cary Eclipse, your computer, monitor, printer or

accessories to the mains power supply until you have made sure that

they are correctly set for the mains power supply in the specific

outlet in your laboratory to which the equipment will be connected.

Consult the manuals supplied with your computer, monitor and

printer for their specific voltage requirements.

Replace blown fuses with fuses of the size and rating as stipulated in

the text adjacent to the fuse holder or in the manuals where listed.

Replace or repair faulty or frayed insulation on power cords.

Do not replace the power cord with one of a lower rating than

specified. Use only Agilent supplied power cords for your country.

Safety Practices and Hazards

10 Cary Eclipse Fluorescence Spectrophotometer User’s Guide

WARNING

Shock Hazard

To avoid electrical shock this equipment must be disconnected from the

mains supply before servicing.

Panels, covers and modules

You are permitted to remove the top colored cover to:



Replace the lamp module.



Adjust the lamp module.

Any other panels or covers, which are retained by screws on the

spectrophotometer and accessories, may be opened ONLY by Agilent-

trained, Agilent-qualified, or Agilent-approved service engineers.

Consult the manuals or product labels supplied with your computer,

monitor and printer to determine which parts are operator-

accessible.

Operators and other unauthorized personnel are permitted access

ONLY to the lamp module and the sample compartment of the Cary

Eclipse. ALWAYS switch off the instrument and disconnect the mains

cord before changing a lamp module.

Other precautions

The lamp module operates at a high temperature, and touching it

may result in burns. Before replacing a lamp module that has been

operating, switch off the Cary Eclipse and ensure that the lamp

module has cooled, or protect your fingers from burns.

Do not block the ventilation grilles on the spectrophotometer and

accessories. Consult the manuals supplied with your computer,

monitor and printer for their specific ventilation requirements.

Use of the Cary Eclipse system and accessories may involve

materials, solvents and solutions, which are flammable, corrosive,

toxic or otherwise hazardous.

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