
Table of contents ■■■■■■■■■■■■■■■■■■■■■■
IV ■■■■■■■■ 889 IC Sample Center
4.3 Full loop injection ............................................................... 21
4.4 Partial loopfill injection ...................................................... 24
4.5 Pickup injection .................................................................. 27
5Handling and maintenance 31
5.1 General ................................................................................ 31
5.2 Care ...................................................................................... 31
5.2.1 Cleaning in general ................................................................ 31
5.3 Maintenance and service ................................................... 32
5.3.1 Sample loop .......................................................................... 32
5.3.2 Replacing the sample needle ................................................. 33
5.3.3 Replacing the air needle ........................................................ 35
5.3.4 Replacing the fuses ................................................................ 36
5.4 Quality Management and validation with Metrohm ....... 37
6Troubleshooting 38
6.1 Error list ............................................................................... 38
6.1.1 Rack unit ............................................................................... 38
6.1.2 Needle unit ............................................................................ 39
6.1.3 Syringe unit ........................................................................... 41
6.1.4 Injection valve unit ................................................................. 42
6.1.5 Cooling unit .......................................................................... 42
6.1.6 Electronics ............................................................................. 43
6.2 Analytical problems ............................................................ 43
6.2.1 Autosampler .......................................................................... 43
7Appendix 46
7.1 Samples and sample vials .................................................. 46
7.2 I/O interface ........................................................................ 46
7.2.1 Properties of the I/O interface ................................................ 47
7.2.2 Pin assignment of the remote interface .................................. 47
8Technical specifications 48
8.1 General ................................................................................ 48
8.2 Sampling .............................................................................. 48
8.3 Analytical characteristics ................................................... 49
8.4 Programming ...................................................................... 49
8.5 Interfaces ............................................................................. 49
8.6 Options (pre-installed) ........................................................ 49
8.7 Mains connection ............................................................... 50
8.8 Safety specifications ........................................................... 50