Hach TPM870 Manuel utilisateur

TPM870 1

TPM870

Turbidity Pump Module

User’s Manual

Manuel d'Utilisation

TPM870 2

D21T069 . Printed by Radiometer Analytical SAS . France . 2008-11C

TPM870 3

General presentation

The TPM870 Turbidity Pump Module is used to interface a turbidimeter

fitted with an analogue measurement output (example the 2100AN IS

turbidimeter from Hach) and a Titration Workstation of the TIM8xx/

TIM9xx range or a ION450/ION570 Ion Analyser.

The TPM870 allows to automate turbidity measurements in association

with pH and conductivity measurements and a potentiometric titration

like water hardness determination for example.

With a PC connected to the Titration Workstation and the TitraMaster 85

PC software, the analysis can be fully automatised and the

measurements collected on the PC.

Présentation générale

Le Module Pompe Turbidité TPM870 est utilisé pour interfacer un

turbidimètre équipé d'une sortie de mesure analogique (exemple : le

turbidimètre 2100AN IS de chez Hach) avec une Station de Titrage de la

gamme TIM8xx/TIM9xx ou un Analyseur d'Ions ION450/ION570.

Le TPM870 permet d'automatiser la mesure de la turbidité en associa-

tion avec la mesure de pH, de conductivité et un titrage potentiométrique

comme la détermination de la dureté de l'eau par exemple.

Avec un PC connecté à la Station de Titrage et le logiciel PC

TitraMaster 85, l'analyse peut être entièrement automatisée et les

mesures récupérées dans le PC.

TPM870 4

ContentsContents

Contents

1. Setting up ....................................................................... 5

1.1 Equipment used ........................................................................ 5

1.2 Hydraulics circuit ...................................................................... 6

1.3 Electrical connections ............................................................... 15

1.4 Preparing the measurement system .......................................... 17

2. Starting an application .................................................. 20

3. Running an analysis ...................................................... 26

4. Recommendations for use and maintenance ............. 29

Appendix A - Technical specifications ................................. 31

Appendix B - The "Selectors" switches ............................... 32

Appendix C - Packing list and accessories ......................... 35

1. Installation et montage .................................................. 37

1.1 Matériel utilisé ........................................................................... 37

1.2 Circuit hydraulique .................................................................... 38

1.3 Connexions électriques ............................................................. 47

1.4 Préparation du système de mesure ........................................... 49

2. Lancement d'une application ....................................... 52

3. Déroulement d'une analyse .......................................... 58

4. Conseils d'utilisation et d'entretien ............................. 61

Annexe A - Caractéristiques techniques ............................. 63

Annexe B - Les interrupteurs "Selectors" ........................... 64

Annexe C - Liste de colisage et accessoires ....................... 67

SommairSommair

Sommairee

TPM870 5

1. Setting up

The TPM870 instrument has been developed to meet the requirements of

electrochemical applications dedicated to water analysis. It is therefore

aimed at experienced users who have the knowledge required to operate

the instrument and implement the security instructions enclosed. We

accept no responsibility for using this measurement system (including

peripheral devices) under conditions that are not specified in this User's

Manual. This system must not, under any circumstances, be used to

perform tests on living beings.

1.1 Equipment used

.A TPM870 Turbidity Pump Module to add turbidity measure

automation to TitraLab or MeterLab system configurations (see table

below), R21T112 (in 230 V) or R21T113 (in 115V).

.A turbidimeter with an analogue measurement output (example:

2100AN IS turbidimeter from Hach).

.A manual Flow Cell Kit for 2100AN IS turbidimeter from Hach.

.< 0.1, 20, 200, 1000, 4000 and 7500 NTU standards.

.A Titration Workstation of the TIM8xx/TIM9xx range or an Ion

Analyser IONxxx. The TIM8xx, TIM9xx or IONxxx used depends on

the applications to be done.

English

ION450 TIM865

TIM9xx

TIM870ION570

pH measurements

Conductivity measurements -

ISE Direct measurements

Potentiometric titrations - -

.A SAC950 sample changer fitted with a 36-position turntable for

180 ml PP sample beakers.

.A PC fitted with TitraMaster 85 Titration Software.

TitraMaster 85, version 5.1.0 or higher.

TPM870 6

00 0

00 0 0 0

Rinsin

Sample

beaker

Waste

1.2 Hydraulics circuit

1.2.1 Operation principle

The sample is driven into the turbidity flow cell (3) with pump (2) after

electrovalve (1) has opened. The sample is evacuated to a waste.

Rinsing water is driven into the turbidity flow cell (3) with pump (2) after

electrovalve (4) has opened. Rinsing water is evacuated to a waste as

for the sample.

Electrovalves (1) and (6) and pump (2) are monitored via the TTL

commands of the instrument used for the electrochemical

measurements. Manual rinse can be triggered by pushing button (5).

TPM870 7

1.2.2 Setting up the hydraulics circuit

We recommend you to place the Hach 2100AN IS turbidimeter onto the

TPM870 and the Titration workstation or Ion Analyser on the left or right

side of these two instruments. The waste and rinse water containers can

be placed on the floor. Have in mind that around 150 ml of rinse water

are required per sample analysis. According to the number of samples to

analyse, it could be interesting to take the rinse water directly from an

ion exchanging column output.

Recommended position and space required

The Sample Changer can be placed on the right or on the left of the

system defined above. Place the extension burette (ABU52 or ABU62)

beside the Titration workstation or Ion Analyser.

TPM870

Turbidimeter

Titration

Workstation

or Ion

Analyser

110 cm

60 cm

English

TPM870 8

1. Setting up the pump head

Mount the peristaltic pump head (1) onto the front panel of the TPM870.

0 0 0

0 0 0 0 0

Pump

Manual Rinse

Power

Sample

Rinse

Turbidity

Meter

Power

Sample

Rinse

Turbidity

Meter

Pump

Manual Rinse

0 0 0

0 0 0 0 0

'Clic'

Pump

Manual Rinse

Power

Rinse Sample

Turbidity

Meter

0 0 0

0 0 0 0 0

Open the pump

TPM870 9

2. Setting up the pump head tubing

Softening silicone tubing (2)

Before a first time use, follow this procedure to soften the silicone

tubing (2) ∅ = 4.8/8.0 mm:

English

Pump

Manual Rinse

Power

Rinse Sample

Turbidity

Meter

Pump

Rinse

Turbidity

Meter

Perform 3 manual rinses

Manual Rinse

Sample

Rinse

Turbidity

Meter

Manual Rinse

Sample

0 0 0

0 0 0 0 0

0 0 0

0 0 0 0 0

Open the pump

Remove the tubing branch

Place this tubing branch

into the pump head and

close the pump

Adjust the tubing diameter

4.8

1.6

TPM870 10

Pump

Rinse

Turbidity

Meter

Perform 3 manual rinses

Manual Rinse

Sample

Rinse

Turbidity

Meter

Manual Rinse

Sample

0 0 0

0 0 0 0 0

Remove the tubing branch

Pump

Manual Rinse

Power

Rinse Sample

Turbidity

Meter

Place the other tubing branch into the pump

head then close the pump

0 0 0

0 0 0 0 0

Open the pump

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