Agilent Technologies AA Series Manuel utilisateur

Agilent 240/280

Series AA

(including Zeeman)

User’s Guide

2 Agilent 240/280 Series AA User’s Guide

Notices

2000-2004, 2010-2012

No part of this manual may be

reproduced in any form or by any

means (including electronic storage

and retrieval or translation into a

foreign language) without prior

agreement and written consent from

Agilent Technologies, Inc. as governed

by United States and international

Manual Part Number

8510154700

Edition

Ninth edition, January 2012

Printed in Malaysia

Agilent Technologies, Inc.

Warranty

The material contained in this

document is provided “as is,” and is

subject to being changed, without

notice, in future editions. Further, to

the maximum extent permitted by

applicable law, Agilent disclaims all

warranties, either express or implied,

with regard to this manual and any

information contained herein,

including but not limited to the

implied warranties of merchantability

and fitness for a particular purpose.

Agilent shall not be liable for errors

or for incidental or consequential

damages in connection with the

furnishing, use, or performance of

this document or of any information

contained herein. Should Agilent and

the user have a separate written

agreement with warranty terms

covering the material in this

document that conflict with these

terms, the warranty terms in the

separate agreement shall control.

Technology Licenses

The hardware and/or software

described in this document are

furnished under a license and may be

used or copied only in accordance

with the terms of such license.

Restricted Rights Legend

If software is for use in the

performance of a U.S. Government

prime contract or subcontract,

Software is delivered and licensed as

“Commercial computer software” as

defined in DFAR 252.227-7014 (June

1995), or as a “commercial item” as

defined in FAR 2.101(a) or as

“Restricted computer software” as

defined in FAR 52.227-19 (June 1987)

or any equivalent agency regulation or

contract clause. Use, duplication or

disclosure of Software is subject to

Agilent Technologies’ standard

commercial license terms, and non-

DOD Departments and Agencies of the

U.S. Government will receive no

greater than Restricted Rights as

defined in FAR 52.227-19(c)(1-2) (June

1987). U.S. Government users will

receive no greater than Limited Rights

as defined in FAR 52.227-14 (June

1987) or DFAR 252.227-7015 (b)(2)

(November 1995), as applicable in any

technical data.

Safety Notices

A CAUTION notice denotes a hazard.

It calls attention to an operating

procedure, practice, or the like that, if

not correctly performed or adhered to,

could result in damage to the product

or loss of important data. Do not

proceed beyond a CAUTION notice

until the indicated conditions are fully

understood and met.

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice, or the

like that, if not correctly performed or

adhered to, could result in personal

injury or death. Do not proceed

beyond a WARNING notice until the

indicated conditions are fully

understood and met.

WARNING

CAUTION

Contents

Agilent 240/280 Series AA User’s Guide 3

Contents

1. Safety Practices and Hazards 7

General 7

Electrical Hazards 8

Heat, Vapors and Fumes 9

Compressed Gases and Cylinders 10

Gas Hoses and Connections 11

Ultraviolet Radiation 11

Other 12

Warning and Caution Messages 12

Warning Symbols 12

Color Coding 14

CE Compliance 15

Electromagnetic Compatibility 15

EN55011/CISPR11 15

ICES/NMB-001 16

Flame Operation 16

Flammable Solvents 16

Compressed Gases and Cylinders for Flame Operation 18

Acetylene 18

Nitrous Oxide 20

Burners 20

Nebulizer 21

Liquid Trap 22

Contents

4 Agilent 240/280 Series AA User’s Guide

Heat Hazards 22

Perchloric Acid 23

Flashbacks 24

Furnace and Zeeman Operation 26

Gases 26

Heat Hazards 26

Vapors and Fumes 27

UV Radiation 27

Magnetic Field (Zeeman only) 27

2. Introduction 29

Installation Requirements 30

Agilent AA Documentation 30

Conventions 30

Specifications 31

Environmental 31

Power 32

Gas supplies 37

Weights and Dimensions 37

3. Installation 39

PC Requirements 39

Recommended PC Configuration 40

Installation Procedure Overview 41

Guidelines for Software Installation 41

Installing the SpectrAA Base Software 42

Installing the SpectrAA PRO Software 45

Contents

Agilent 240/280 Series AA User’s Guide 5

Installing the SpectrAA CFR Software 47

Installing the SpectrAA Base Software 47

Installing the SpectrAA CFR Software 50

GPIB Communications 51

Installing the PCI-GPIB Communications Card 51

Configuring the PCI-GPIB Communications Card 54

Installing the USB-GPIB-HS Converter 55

Setting Up for Agilent AA-DUO Operation 55

Starting the SpectrAA Software 56

SpectrAA Release Notes and Software Status Bulletin 57

Installing the Drivers for the Tube-CAM Furnace Camera Option 57

Driver Installation 58

Printer Setup 60

Troubleshooting 60

4. Software Overview 61

Starting the SpectrAA Software 62

SpectrAA Windows 62

Index Page 62

Worksheet Window 63

Reports Window 65

Administration Window 66

Working With the SpectrAA Software 67

Menu Bar 67

Toolbar 67

Dialog Boxes 67

Contents

6 Agilent 240/280 Series AA User’s Guide

Help 67

Searching for Help 68

Printing Help 69

Viewing Help While You Work 69

Quitting Help 69

5. Getting Started 71

Instrument Setup 71

Connections 72

Power 72

Moving Your Instrument 73

Starting the System 73

Pre-analysis Checklist 74

Safety Practices and Hazards

Agilent 240/280 Series AA User’s Guide 7

1. Safety Practices and Hazards

General 7

Electrical Hazards 8

Heat, Vapors and Fumes 9

Compressed Gases and Cylinders 10

Gas Hoses and Connections 11

Ultraviolet Radiation 11

Other 12

Warning and Caution Messages 12

Warning Symbols 12

Color Coding 14

CE Compliance 15

Electromagnetic Compatibility 15

Flame Operation 16

Flashbacks 24

Furnace and Zeeman Operation 26

General

Your Agilent AA instrument and accessories have been carefully

designed so that when used properly you have an accurate, fast,

flexible and safe analytical system.

If the equipment is used in a manner not specified by the

manufacturer, the protection provided by the equipment may be

impaired.

Safety Practices and Hazards

8 Agilent 240/280 Series AA User’s Guide

Operation of an atomic absorption spectrometer can involve the use

of compressed gases, flames, and hazardous materials including

corrosive fluids and flammable liquids. Unskilled, improper, or

careless use of this instrument can create explosion hazards, fire

hazards, or other hazards which can cause death, serious injury to

personnel, or severe damage to equipment and property.

Information on safety practices is provided with your instrument and

operation manuals, and also referenced in your Agilent accessory

manuals. Before using your instrument or accessories, you must

thoroughly read these safety practices.

Observe all relevant safety practices at all times.

The safety practices described below are provided to help you

operate the instrument safely. Read each safety topic thoroughly

before attempting to operate the instrument and always operate the

spectrometer in accordance with these safety practices.

Electrical Hazards

The instrument and accessories contain electrical circuits, devices

and components operating at dangerous voltages. Contact with these

circuits, devices and components can cause death, serious injury, or

painful electric shock.

Panels and covers that are retained by fasteners which require the

use of a tool for removal may only be opened by Agilent field service

engineers. Consult the manuals or product labels supplied with your

PC, monitor, printer/plotter, water-cooling system and vacuum pump

(where required) to determine which parts are operator-accessible.

Application of the wrong supply voltage, connection of the

instrument to an incorrectly wired supply outlet, or lack of proper

electrical grounding can create a fire hazard or a potentially serious

shock hazard, and could seriously damage the instrument and any

attached ancillary equipment.

Always use a 3-wire outlet with ground connection which is

adequately rated for the load. The installation must comply with local

and national safety regulations.

Safety Practices and Hazards

Agilent 240/280 Series AA User’s Guide 9

Do not connect the instrument to the mains power supply until you

have made sure that the operating voltage is correctly set for the

mains power supply in the specific outlet in your laboratory to which

the equipment is connected.

Heat, Vapors and Fumes

Heat, vapors and fumes generated by flame, furnace and vapor

generation methods can be hazardous to personnel.

Heat, vapors and fumes must be extracted from the instrument by an

exhaust system. The instrument must be vented into a self-contained

arrangement of collector hood, ducting and exhaust fan. The system

must be vented to the outside air, never within the building. Locate

the system outlet such that the exhaust cannot re-enter the building

through any door, window, air conditioning inlet, or other ventilator.

Construct the system in accordance with local codes and regulations

for ventilation.

The exhaust system must be capable of providing an exhaust

ventilation rate of at least 6 cubic meters per minute (200 cfm).

Locate the exhaust fan at least 3 meters (10 feet) away from the

flame and as close to the outlet as possible. The motor must be

mounted away from the hot gases, and plastic parts must not be used

as they will melt. Fit a back-draft damper to the outlet end of the

system. Equip the exhaust fan power supply with an indicator close

to the instrument to indicate whether the exhaust fan is on or off.

Always switch the exhaust fan on before lighting the flame.

Use fireproof ducting that is in accordance with your local fire

prevention regulations. Locate the ducting away from fire alarms,

sprinkler heads and other heat-sensitive devices. Do not make solder

joints in the ducting—the hot exhaust in the duct may melt the joint.

Regularly check the system by smoke test to ensure that the exhaust

system is working.

When operating the atomic absorption spectrometer, always have the

chimney in place to ensure correct ventilation.

Safety Practices and Hazards

10 Agilent 240/280 Series AA User’s Guide

Compressed Gases and Cylinders

All compressed gases (other than air) can create a hazard if they leak

into the atmosphere. Even small leaks in gas supply systems can be

dangerous. Any leak (except that of air) can an explosion hazard, a

fire hazard, or result in an oxygen–deficient atmosphere. Such

hazards can cause death, serious injury, asphyxiation, anesthetic

effects, and serious damage to equipment and property.

Cylinders must be stored and handled strictly in accordance with

local safety codes and regulations. Cylinders must be used and stored

only in a vertical position. Secure all cylinders to an immovable

structure or a properly constructed cylinder stand. The area in which

cylinders are stored must be adequately ventilated to prevent toxic or

explosive accumulations. Move cylinders only on a properly

constructed trolley.

Keep cylinders cool. This rule applies to every cylinder of

compressed gas. Cylinders have pressure relief devices that release

the contents of the cylinder if the temperature exceeds 52 °C

(125 °F).

Ensure that all cylinders are clearly labeled so that there can be no

doubt about the contents. If the cylinder label is not legible, do not

use the cylinder—return it to your supplier. Always ensure that you

have the right cylinder before connecting the cylinder to the

instrument.

If air is supplied from a compressor, all moisture must be extracted

from the air before it is supplied to the gas control module. Moisture

can affect the internal components of the gas control system and

create a potentially hazardous situation.

Use only approved regulators and hose connectors.

Never attempt to refill cylinders.

Remember that for cylinder connections, left-hand thread fittings are

used for fuel; right-hand thread fittings are used for support gases.

When your analytical program is complete, or at the end of the

working day, always ensure that all gas supplies are turned off at the

cylinders.

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