Shimadzu PDA-7000 Manuel utilisateur

211-78001E

Jun. 2018

SHIMADZU OPTICAL EMISSION SPECTROMETER

PDA-7000

INSTRUCTION MANUAL

Read the instruction manual thoroughly before you use the product.

Keep this instruction manual for future reference.

* Refer to the following document for detailed operation of software.

Data Processing Software PDAfor Windows Operatioin Manual

P/N 211-54796

Data Processing Software PDA for Windows Installation Manual

P/N 211-78114

ANALYTICAL & MEASURING INSTRUMENTS DIVISION

(This page is intentionally left blank.)

Introduction

Read this Instruction Manual thoroughly before using the product.

Thank you for purchasing Shimadzu optical emission spectrometer PDA-7000.

PDA-7000 is a PDA photoelectric-photometric optical emission spectrometer which

simultaneously and quickly carries out analyses of multi-elements in metal with a high

precision. The photoelectric-photometric emission spectrometer, which is adopted in a

wide range of fields, is an essential instrument for quality control.

This manual describes the installation, operation, usage cautions, accessories and

options for this product. Read this manual thoroughly before using the product and

operate the product in accordance with the instructions in this manual.

Also, keep this manual for future reference.

IMPORTANT

•If the user or usage location changes, ensure that this Instruction Manual is always

kept together with the product.

•If this manual or a product warning label is lost or damaged, immediately contact

your Shimadzu representative to request a replacement.

•To ensure safe operation, read all Safety Instructions before using the product.

•To ensure safe operation, contact your Shimadzu representative if product

installation, adjustment, or re-installation (after the product is moved) is required.

Notice

•Information in this manual is subject to change without notice and does

not represent a commitment on the part of the vendor.

•Any errors or omissions which may have occurred in this manual despite

the utmost care taken in its production will be corrected as soon as

possible, although not necessarily immediately after detection.

•All rights are reserved, including those to reproduce this manual or parts

thereof in any form without permission in writing from Shimadzu

Corporation.

•Microsoft and Windows are registered trademarks of Microsoft

Corporation in the United States and/or other countries. Other company

names and product names mentioned in this manual are trademarks or

registered trademarks of their respective companies.

The TM and ® symbols are omitted in this manual.

iii

Indications Used in This Manual

Dangers, Warnings, Cautions, and Notes are indicated using the following conventions:

Note

Dangers, Warnings, Cautions, and Notes are indicated using the

following conventions:

Warning

Indicates a potentially hazardous situation which, if not

avoided, could result in serious injury or possibly

death.

Caution

Indicates a potentially hazardous situation which, if not

avoided, may result in minor to moderate injury, or

equipment damage.

Note

Emphasizes additional information that is provided to

ensure the proper use of this product.

Warning Labels

Warning

Electric Shock

Before removing the excitation unit front panel, be sure to turn OFF

the power of the excitation source unit. Never remove other panels.

Front Panel of Excitation Unit

Safety Instructions

To ensure safe product operation, read these important safety instructions carefully before

use and follow all DANGER, WARNING and CAUTION instructions given in this section.

Installation Site

Warning

Do not operate PDA-7000 under explosive and/or corrosive

atmosphere.

Note

When installing PDA-7000 near apparatus generating a ferromagnetic

field such as an electric arc furnace, contact your Shimadzu

representative.

Installation

To ensure safe operation, contact your Shimadzu representative if product installation,

adjustment, or re-installation (after the product is moved) is required.

Operation

PDA-7000 generates high voltage based on the measurement principles. If it is correctly

used, no problem will occur. If not, it may cause an accident and damage. For safety

operation and dangerous accident prevention, strictly observe the following precautions.

1. Precautions for operator safety and for handling the instrument

Warning

PDA-7000 may cause radio disturbance during discharge. Personnel

with pacemakers should be especially careful during discharge.

Caution

Electric Shock

Never start the discharge without correctly setting and holding the

sample on the spark stand.

Caution

●Thoroughly read the instruction manual to strictly observe it. If you

have any question, contact your Shimadzu representative.

●Keep this instruction manual near the instrument for quick

reference of the operation procedures and safety precautions

anytime necessary.

Note

The contents of the hard disk of the personal computer may be lost as

the result of an unforeseen accident. Always create a backup to

protect critical data from such accidents.

vii

2. Restriction of operators

Warning

The inside of the instrument should only be repaired by personnel

specially trained by Shimadzu Corporation since it is dangerous. Do

not disassemble or modify the instrument without permission as it

may compromise the safety of the instrument.

Caution

Use of the instrument is allowed only to personnel who have

understood the safety precautions well and have been well-trained for

the operating procedure.

It is a must to establish a system by which no one other than the

operator above is allowed to use it.

viii

In an emergency

Warning

●In case of leakage of argon gas

If it is left, lack of oxygen may occur. Immediately ventilate the

working area and check for gas piping.

●In case of abnormal temperature raise of the spectrometer unit

The room temperature should be kept within the range of 10 - 28°C.

If it exceeds 30°C, the temperature of the spectrometer unit may

raise abnormally.

If the temperature of the spectrometer unit exceeds 42°C, the buzzer

at the temperature alarm will give a warning sound. In that case,

turn OFF the AIRCON switch on the switch panel and make sure the

room temperature is within the range of 10 - 28°C. Then, wait until

the temperature inside the spectrometer goes down to the room

temperature, and turn ON the AIRCON switch again.

If the buzzer gives a warning sound even after that, turn OFF the

AIRCON switch and contact your Shimadzu representative.

●Safety measure for other emergency occurrences

If an unpredictable happening like an earthquake, fire, etc. occurs,

first press the emergency stop switch, and then turn OFF all the

power of the distribution panel. After this, each staff must carefully

take an appropriate action to maintain his/her safety.

During a power outage

In case of a power failure, follow the procedure described below.

1. Turn off the MAIN breaker on the switch panel.

2. Turn off theAIRCON, CONSOLE, and SOURCE switches on the switch panel.

3. Turn off the power switch of the vacuum pump.

4. When the power is back, turn on the MAIN breaker on the switch panel.

5. Turn on the AIRCON, CONSOLE, and SOURCE switches on the switch panel.

6. Turn on the power of the vacuum pump.

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