Horiba F-74BW Manuel utilisateur

Instruction Manual

pH/ION/COND METER

F-74BW

表紙は別途デザインの表紙とする

■Preface

This manual describes the operation of the F-74BW pH/ION/COND Meter.

Be sure to read this manual before using the product to ensure proper and safe

operation of the instrument. Also safely store the manual so it is readily available

whenever necessary.

Product specifications and appearance, as well as the contents of this manual

are subject to change without notice.

■Warranty and Responsibility

HORIBA, Ltd. warrants that the Product shall be free from defects in material

and workmanship and agrees to repair or replace free of charge, at option of

HORIBA, Ltd., any malfunctioned or damaged Product attributable to

responsibility of HORIBA, Ltd. for a period of one (1) year from the delivery

unless otherwise agreed with a written agreement. In any one of the following

cases, none of the warranties set forth herein shall be extended;

・Any malfunction or damage attributable to improper operation

・Any malfunction attributable to repair or modification by any person not

authorized by HORIBA, Ltd.

・Any malfunction or damage attributable to the use in an environment not

specified in this manual

・Any malfunction or damage attributable to violation of the instructions in this

manual or operations in the manner not specified in this manual

・Any malfunction or damage attributable to any cause or causes beyond the

reasonable control of HORIBA, Ltd. such as natural disasters

・Any deterioration in appearance attributable to corrosion, rust, and so on

Replacement of consumables

HORIBA, LTD. SHALL NOT BE LIABLE FOR ANY DAMAGES RESULTING

FROM ANY MALFUNCTIONS OF THE PRODUCT, ANY ERASURE OF DATA,

OR ANY OTHER USES OF THE PRODUCT.

■Trademarks

Generally, company names and brand names are either registered trademarks

or trademarks of the respective companies.

■Unauthorized Reprinting or Copying of This

Operation Manual

No unauthorized reprinting or copying of all or part of this operation manual is

allowed. The utmost care has been used in the preparation of this operation

manual.

REGULATIONS

■Conformable Directive

This equipment conforms to the following directives and standards:

●Installation Environment

This product is designed for the following environment.

- Overvoltage category II

- Measurement category I

WARNING: Do not use the equipment for measurements within

measurement categories II, III and IV.

●Information on Disposal of Electrical and Electronic Equipment and

Disposal of Batteries and Accumulators

REGULATIONS

Directives: The EMC Directive 2004/108/EC

The Low Voltage Directive 2006/95/EC

Standards: [the EMC Directive] EN61326-1:2006

Class B, Basic requirements

[the Low Voltage Directive] EN61010-1:2010(Ed.3.0)

The crossed out wheeled bin symbol with underbar shown on the

product or accompanying documents indicates the product requires

appropriate treatment, collection and recycle for waste electrical and

electronic equipment (WEEE) under the Directive 2002/96/EC, and/or

waste batteries and accumulators under the Directive 2006/66/EC in

the European Union.

The symbol might be put with one of the chemical symbols below. In

this case, it satisfies the requirements of the Directive 2006/66/EC for

the object chemical.

This product should not be disposed of as unsorted household waste.

Your correct disposal of WEEE, waste batteries and accumulators will

contribute to reducing wasteful consumption of natural resources, and

protecting human health and the environment from potential negative

effects caused by hazardous substance in products.

Contact your supplier for information on applicable disposal methods.

REGULATIONS

■FCC Rules

Any changes or modifications not expressly approved by the party

responsible for compliance shall void the user's authority to operate the

equipment.

●WARNING

This equipment has been tested and found to comply with the limits for

a Class A digital device, pursuant to part 15 of the FCC Rules. These

limits are designed to provide reasonable protection against harmful

interference when the equipment is operated in a commercial

environment. This equipment generates, uses, and can radiate radio

frequency energy and, if not installed and used in accordance with the

instruction manual, may cause harmful interference to radio

communications.

Operation of this equipment in a residential area is likely to cause

harmful interference in which case the user will be required to correct

the interference at his own expense.

SAFETY OPERATION

III

■Hazard Classification and Warning Symbols

Warning messages are described in the following manner. Read the

messages and follow the instructions carefully.

●Hazard classification

●Warning symbols

SAFETY OPERATION

This indicates an imminently hazardous situation which, if not

avoided, will result in death or serious injury. This signal word

is to be limited to the most extreme situations.

This indicates a potentially hazardous situation which, if not

avoided, could result in death or serious injury.

This indicates a potentially hazardous situation which, if not

avoided, may result in minor or moderate injury. It may also be

used to alert against unsafe practices.

Without safety alert indication of hazardous situation which, if

not avoided, could result in property damage.

Description of what should be done, or what should be followed

Description of what should never be done, or what is prohibited

SAFETY OPERATION

■Safety Precautions

This section provides precautions to enable you to use the product

safely and correctly and to prevent injury and damage. The terms of

DANGER, WARNING, and CAUTION indicate the degree of imminency

and hazardous situation. Read the precautions carefully as it contains

important safety messages.

WARNING

Do not use an unspecified AC adapter.

Otherwise, it may heat up or be ignited resulting in a fire or an accident.

Do not disassemble or modify the meter.

Otherwise, it may heat up or be ignited resulting in a fire or an accident.

CAUTION

Harmful chemicals

Some ion electrodes are used with hazardous standard solutions. Handle them

with care.

If the internal solution comes in contact with the skin, wash it off immediately. If it

gets into eyes, flush with plenty of water and then consult a doctor.

Harmful chemicals

The internal solution of an electrodes is highly concentrated potassium chloride

(3.33 mol/L KCl).

If the internal solution comes in contact with the skin, wash it off immediately. If it

gets into eyes, flush with plenty of water and then consult a doctor.

Broken glass

Broken glass may cause injury.

The outer tube and tip of an electrode are made of glass.

Handle them with care.

Do not use the cable of serial communication, USB, or AC adapter under wet or

humid conditions.

Otherwise, it may cause an fire, electric shock, or breakage.

SAFETY OPERATION

■Product Handling Information

●Operational Precautions

●Do not drop, crash, or give any physical impact on the instrument.

●Do not immerse the instrument into alcohol, organic solvent, strong

acid, strong alkaline, or the like. The instrument body contains ABS

resin, acrylic resin, and some rubber parts.

●If the instrument is dropped into water or gets wet, wipe it using soft

cloth. Do not heat to dry it with a hair-dryer (or the like).

●Use fingers to press the operation keys or the touch panel.

Do not use a hard object like a metal stick or rod.

●Be careful not to let water into the instruction inside.

The instrument is not water-proof.

●To disconnect an electrode or interface cable, hold the connector and

pull it off. If you pull at the cable, it may cause a breakage.

●The touch panel is capacitance-type. Make sure to turn OFF the

power before cleaning the panel. If you wipe it with the power ON, it

may cause instrument malfunction.

●RS-232C or USB communication between the instrument and a per-

sonal computer may fail because of environmental conditions, such

as (radio/electromagnetic) noise.

●Environmental conditions for use and storage

●Temperature: 0°C to 45°C

●Humidity: under 80% in relative humidity and free from

condensation

Avoid the following conditions:

●Dusty environment

●Strong vibration

●Direct sunlight

●Corrosive gas environment

●Close to an air-conditioner

●Direct wind

●Transportation

When transporting the instrument, repackage it in the original package

box. Otherwise, it may cause instrument breakage.

●Disposal

Standard solution used for the calibration must be under neutralized

before the disposal. As for the disposal of the meter, treat it as an

industrial waste.

MANUAL INFORMATION

■Description in This Manual

This interprets the necessary points for correct operation and notifies

the important points for handling the instrument.

This indicates the part of where to refer the informatione.

This indicates reference information.

MANUAL INFORMATION

HINT!

CONTENTS

VII

Chapter 1 About the F-74BW . . . . . . . . 1

Chapter 2 Information of the F-74BW . 2

2.1 Measurement Items . . . . . . . . . . . . . . . . . . . . . . . 2

2.2 Packing List . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3

2.3 Names and Functions . . . . . . . . . . . . . . . . . . . . . 4

2.3.1 Names of Each Part . . . . . . . . . . . . . . . . . . . . . . . . . . 4

2.3.2 Display . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5

2.3.3 Operation Key . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6

2.4 Measurement (MEAS) Flow Chart . . . . . . . . . . . . 7

2.4.1 CH1 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7

2.4.2 CH2 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7

2.5 Setting (SET) Flow Chart . . . . . . . . . . . . . . . . . . . 8

2.5.1 CH1 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8

2.5.2 CH2 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9

2.6 Data (DATA) Flow Chart . . . . . . . . . . . . . . . . . . . 10

Chapter 3 Basic Operation . . . . . . . . . 11

3.1 Preparation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11

3.1.1 Assembling the Electrode Stand . . . . . . . . . . . . . . . 11

3.1.2 Electrode Connection . . . . . . . . . . . . . . . . . . . . . . . . 12

3.1.3 Connecting the Power Source . . . . . . . . . . . . . . . . . 13

3.1.4 Connecting and Setting the Printer . . . . . . . . . . . . . 14

3.1.5 Connecting the Personal Computer . . . . . . . . . . . . . 15

3.2 Settings . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16

3.2.1 pH Standard Solution Setting . . . . . . . . . . . . . . . . . . 16

3.2.2 Temperature Compensation Function Setting . . . . . 18

3.2.3 Auto Data Memory Setting . . . . . . . . . . . . . . . . . . . . 20

3.2.4 pH Calibration Interval Setting . . . . . . . . . . . . . . . . . 21

3.2.5 Sample ID Setting . . . . . . . . . . . . . . . . . . . . . . . . . . 22

3.2.6 ION Unit Setting . . . . . . . . . . . . . . . . . . . . . . . . . . . . 23

3.2.7 ION Valency Setting . . . . . . . . . . . . . . . . . . . . . . . . . 24

3.2.8 Conductivity Unit Setting . . . . . . . . . . . . . . . . . . . . . 25

CONTENTS

VIII

3.2.9 Conductivity

Temperature Coefficient Setting . . . . . . . . . . . . . . . 26

3.2.10 Conductivity Cell Constant Setting . . . . . . . . . . . . . 27

3.2.11 Salinity Unit Setting . . . . . . . . . . . . . . . . . . . . . . . . 28

3.2.12 Auto Printer Setting . . . . . . . . . . . . . . . . . . . . . . . . 29

3.2.13 Maintenance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 30

3.3 Calibration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 45

3.3.1 pH Calibration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 45

3.3.2 ION Calibration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 54

3.3.3 Conductivity Calibration . . . . . . . . . . . . . . . . . . . . . . 66

3.3.4 Salinity Calibration . . . . . . . . . . . . . . . . . . . . . . . . . . 67

3.3.5 Calibration Value Printing . . . . . . . . . . . . . . . . . . . . . 69

3.4 Measurement . . . . . . . . . . . . . . . . . . . . . . . . . . . 71

3.4.1 Measurement Value Hold . . . . . . . . . . . . . . . . . . . . . 71

3.4.2 Measurement Items Changing . . . . . . . . . . . . . . . . . 72

3.4.3 Auto Data Memory . . . . . . . . . . . . . . . . . . . . . . . . . . 73

3.4.4 Measurement Value Printing . . . . . . . . . . . . . . . . . . 74

3.5 Data Operation . . . . . . . . . . . . . . . . . . . . . . . . . . 78

3.5.1 Data Memory of Measurement Value . . . . . . . . . . . 78

3.5.2 Memory Data Display . . . . . . . . . . . . . . . . . . . . . . . . 79

3.5.3 Memory Data Printing . . . . . . . . . . . . . . . . . . . . . . . 80

3.5.4 Calibration History Display . . . . . . . . . . . . . . . . . . . . 82

3.5.5 Calibration History Printing . . . . . . . . . . . . . . . . . . . . 84

3.5.6 pH Check History Display . . . . . . . . . . . . . . . . . . . . 86

3.5.7 pH Check Data Printing . . . . . . . . . . . . . . . . . . . . . . 87

Chapter 4 Maintenance and

Troubleshooting . . . . . . . . 88

4.1 pH (ORP) Electrode Maintenance . . . . . . . . . . . 88

4.2 ION Electrode Maintenance . . . . . . . . . . . . . . . 92

4.2.1 65XX-10C Electrode Maintenance . . . . . . . . . . . . . . 94

4.3 Conductivity Electrode Maintenance . . . . . . . . 99

4.4 Troubleshooting . . . . . . . . . . . . . . . . . . . . . . . . 100

4.4.1 Error Message Chart . . . . . . . . . . . . . . . . . . . . . . . 100

4.4.2 More Troubleshooting . . . . . . . . . . . . . . . . . . . . . . 107

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