Table of Contents
1Contact information .............................................................................................................................. 6
2Notes on the Manual ............................................................................................................................. 6
2.1Explanations of the Safety Instructions ............................................................................................. 7
2.2 General Safety Instructions ............................................................................................................... 9
2.3 Explanation of signs and symbols ................................................................................................... 10
3Packaging, Transport and Installation .............................................................................................. 11
3.1 Packaging........................................................................................................................................ 11
3.2 Transport.......................................................................................................................................... 11
3.3 Intended use.................................................................................................................................... 11
3.4 Conditions for the Installation Site................................................................................................... 11
3.5 Type Plate Description..................................................................................................................... 12
4Installation............................................................................................................................................ 13
4.1 Setting check up .............................................................................................................................. 13
4.2 Front panel illustration ..................................................................................................................... 14
4.3 Mains power connections................................................................................................................ 15
4.4 Data Interface .................................................................................................................................. 16
4.5 Gas connections.............................................................................................................................. 17
4.6 Gas purification furnance connecting (optional).............................................................................. 18
4.7 Autoloader (optional) ....................................................................................................................... 19
5Analysis................................................................................................................................................ 20
5.1 Working procedure .......................................................................................................................... 20
5.2 Analysis example............................................................................................................................. 22
5.2.1 Combustion peak......................................................................................................................... 22
5.2.2 Combustion double peak............................................................................................................. 22
5.3 Work breaks..................................................................................................................................... 23
5.4 Crucibles preheating, optional......................................................................................................... 23
5.4.1 Operating the pre-heating furnace (optional)............................................................................... 24
5.5 Applications...................................................................................................................................... 24
6Maintenance......................................................................................................................................... 29
6.1 General information ......................................................................................................................... 29
6.1.1 Maintenance every 100 analyses:............................................................................................... 29
6.1.2 Maintenance every 500 analyses:............................................................................................... 29
6.1.3 Maintenance every 1000 analyses:............................................................................................. 29
6.1.4 Maintenance every 2000 analyses:............................................................................................. 29
6.2 Reagent tubes –removing and installing ........................................................................................ 30
6.3 Reagent tubes filling ........................................................................................................................ 32
6.3.1 Chemicals.................................................................................................................................... 32
6.3.2 Reagent tube filling...................................................................................................................... 34
6.3.3 Oxygen purification furnace quartz tube filling (optional) ............................................................ 37
6.3.4 Halogen trap filling (optional)....................................................................................................... 38
6.3.5 Paper filter changing.................................................................................................................... 40
6.4 O-rings replacement........................................................................................................................ 41
6.4.1 Replacing the o-rings 11 and 12 for combustion tube:................................................................ 42
6.4.2 Replacing the o-ring 13 for lower furnace lock ............................................................................ 42
6.4.3 Replacing the o-rings for furnace seal......................................................................................... 43
6.5 Furnace cleaning brush - replacing ................................................................................................. 44
6.6 Dust trap cleaning............................................................................................................................ 45
6.6.1 Fast filter cleaning........................................................................................................................ 46
6.6.2 Thorough cleaning....................................................................................................................... 47
6.7 Oxygen purification furnace refilling ................................................................................................ 48
6.8 Combustion tube replacement......................................................................................................... 49
6.9 Generator tube replacing................................................................................................................. 51
