Buchi Syncore Manuel utilisateur
Operation Manual
Platform
Sy
ncore®
093008 en
Syncore Platform
3
Table of contents
Table of contents
en, Version E (43 pages) Order code
Syncore Instructions 093008
1 Scope of delivery 2
2 Safety 6
3 Function 10
3.1 The single platform 10
3.2 Syncore Analyst R-4, R-6 and R-12 11
3.3 Individual components 11
3.4 Syncore Polyvap R-4 to R-96 12
4 Putting into operation 14
5 Operation 17
5.1 The single platform 17
5.2 Safety instructions 17
5.3 Temperature and RPM 19
5.4 Programm mode: Temperature / Time steps 20
5.5 Further control parameters 22
5.6 Pre-set safety settings 23
5.7 Overview of switches 24
5.8 Signal outlets 25
5.9 After running of the programmable valve 26
5.10 RS-232 interface 26
5.11 Signal inlets 27
5.12 Adjusting the eccentricity 28
5.13 Unbalance compensation 30
5.14 Troubleshooting: the single platform 33
6 Maintenance 34
6.1 Cleaning 34
6.2 Routine inspection of the equipment (monthly) 34
6.3 Routine inspection of the equipment (annually) 35
6.4 Calibration 35
6.5 Error messages: Calibration 37
6.6 Replacement of the fuses 37
6.7 Error Messages: Hardware 38
6.8 Customer service 38
7 Taking out of Operation 39
8 Replacement Parts 40
8.1 Single platform 40
9 Appendix 41
9.1 Technical data 41
9.2 Materials used 41
9.3 FCC requirements (for USA and Canada) 42
9.4 Declaration of conformity 43
Read this Operation Manual through care-
fully before starting to use the Syncore
Product Line.
Always keep these instructions ready at
hand close to the equipment so that they
may be consulted quickly at all times. Chap-
ter 2 provides important safety instructions
that must be followed to ensure safe ope-
ration of the unit.
We reserve the right to make technical changes without
prior notice. No portions of this Operation Manual may be
reproduced in any form (including with the use of electronic
or optical systems), duplicated, or distributed without written
permission from BÜCHI Labortechnik AG. All rights reserved.
Copyright © BÜCHI Labortechnik AG 2013
Syncore Platform
4
1 Scope of delivery
Figure 1: BUCHI Syncore Analyst R-6
Voltage
1 100V 50/60Hz
2 120V 50/60Hz
3 230V 50/60Hz
Condenser
0 None
S Type S, Standard
C Type C, Cold trap
Round receiving flask,
KS 24/20,PLG
0 None
2 2000ml total volume
Rack type (incl. vacuum
cover)
4 Crystal Rack R-4 Analyst
5 Crystal Rack R-6 Analyst
6 Rack R-12 Analy
Residual volume of glass
tubes
4 1ml
5 0.3ml
6 3ml
Glass tube graduation
Y Yes
N No
1 Power system cable PNE, 1.5 m
Type CH 10010
Type Schuko 10016
Type GB 17835
Type USA 10020
Type AUS 17836
1 Scope of delivery
1.1 Configuration Syncore Analyst
1A 0
in addition:
2 Cooling hoses, 1m 04133
1 Power system cable PNE, 1.5m
Type CH 10010
Type Schuko 10016
Type GB 17835
Type USA 10020
Type AUS 17836
1 Operation Manual:
German 93007
English 93008
French 93009
Italian 93010
Spanish 93011
Syncore Platform
5
1 Scope of delivery
Figure 2: BUCHI Syncore Polyvap R-24
1.2 Configuration Syncore Polyvap
1 Power system cable PNE, 1.5 m
Type CH 10010
Type Schuko 10016
Type GB 17835
Type USA 10020
Type AUS 17836
1 Operation Manual:
German 93007
English 93008
French 93009
Italian 93010
Spanish 93011
1P 000
Voltage
1 100V 50/60Hz
2 120V 50/60Hz
3 230V 50/60Hz
Condenser
0 None
S Type S, Standard
C Type C, Cold trap
Round receiving flask,
KS 24/20,PLG
0 None
1 1000ml total volume
2 2000ml total volum
Rack type (incl. vacuum cover)
0 None
1 Crystal Rack R-4
2 Crystal Rack R-6
3 Rack R-12
4 Standard Rack R-24
5 Falcon Rack R-24
6 Rack R-96
in addition:
Syncore Platform
6
1 Scope of delivery
Figure 3: Syncore single platform
1.3 Individual components
Single Platform
Components Order code
Syncore Single Platform 230 V 50/60 Hz 38429
Syncore Single Platform 120 V 50/60 Hz 38430
Syncore Single Platform 100 V 50/60 Hz 38431
Scope of delivery
1 Syncore Single Platform, complete Including:
1 Adjustment wrench for adjusting eccen- 38477
tricity and unbalance compensation
1 Power system cable PNE, 1.5 m
Type CH 10010
Type Schuko 10016
Type GB 17835
Type USA 10020
Type AUS 17836
1 Operation Manual:
German 93007
English 93008
French 93009
Italian 93010
Spanish 93011
Table 4: Individual components single platform
Syncore Platform
7
2 Safety
2 Safety
This unit and all its components have been built in accor-
dance with the state of the art and recognized safety rules.
Nevertheless, certain risks and dangers may be involved
when working with the unit or its individual components:
• Whenevertheunitisnotbeingusedinaccordancewith
its intended purpose, or
• Wheneverthestaffoperatingtheunithavenotlacksuf-
ficient training and know-how.
2.1 Symbols
Stop
Information on hazards that can result in severe material da-
mage or serious to fatal injuries.
Warning
Information on hazards that can result in injury to one’s health
or material damage.
Caution
Information pointing out technical requirements. A failure to
follow these instructions can cause malfunctions, unecono-
mical operation, and production losses.
2.2 Requirements for the user
This unit and all accessories for the Syncore line of equipment
may be used only by laboratory staff and other individuals
who, based on their education, training, or professional
experience, are fully aware of the risks involved in their use.
Staff lacking this training or staff currently being trained need
careful instruction. These operating instructions are valid as
a basic requirement.
Syncore Platform
8
2 Safety
2.3 Authorized use
This unit has been designed and built as a laboratory
instrument. The authorized application for the Syncore single
platform inconjunction with accessories from the Syncore
product line is as follows:
Syncore Polyvap/Syncore single platform
with accessories:
• Parallelevaporation of solvents invarious formats and
containers across a range of temperatures from room
temperature up to + 150 °C and within a range of pres-
sures from 1 mbar up to ambient pressure.
Syncore Analyst:
• Parallelconcentrationofsolventsfrom6differentsamples
across a range of temperatures from room temperatures
up to + 100 ° (or bypassing pre-set safety settings, up to
150 °C), within a range of pressures from 1 mbar up to
ambient pressure.
Applications for the Syncore line of equipment
include:
• Parallelorganic-inorganicchemicalsynthesisintheliqui-
dor in the solid phase.
• Parallelmaterialinvestigations,digestions,preparationof
samples of from 4 to 96 samples, with sample volumes
ranging from 500 down to 1 ml.
• Parallelevaporationoffrom4to96sampleswithsample
volumes from 1 ml up to 500 ml after chemical synthesis,
after chromatography, after extraction, etc.
• Parallelconcentrationinchemicalanalysis,guaranteeing
a residual volume after the evaporation.
2.4 Unauthorized use
Any use other than those indicated above and any application
that does not correspond to the Technical Data is considered
to be improper use.
If the equipment is used in a manner not specified by the
manufacturer, the protection provided by the equipment
may be impaired.
The operator himself bears sole responsibility for any risks
arising from such use.
The following in particular are explicitly forbidden:
• The processing of samples that can explode or ignite
explosively as the result of impact, friction, heat, or spar-
king (e.g., explosives, etc.).
• Thecarryingoutofchemicalreactionsthatcanproduce
substances that can explode or ignite explosively as the
resultof impact, friction, heat, or sparking (e.g., explosives,
etc.);
• Use of the unit in rooms that require explosion-proof
equipment;
Syncore Platform
9
2 Safety
Symbol Meaning Location
Elemento caliente,
superficie caliente
General warning
• Useofthesingleplatformwithsampleholdersorsample
containers that have not been developed for use on the
Syncore single platform.
• Workingataboveatmosphericpressure
2.5 Basic hazards
The basic hazards arise from:
• Chemicals that are toxic or cause allergic reactions, or
can, in a chemical reaction, produce compounds that are
toxic or cause allergic reactions;
• Solventmaterialswhichcanformperoxides
• Veryhotorverycoldpartsmadeofplasticsandmetals
(Burn injuries)
• Kinkedhosesorthedissolvingofhosematerialsusedto
introduce liquids, compressed gases under pressure
• Movingpartswhichrotateathighspeedaboutanaxisand
which if used in an improper way can lead to injury or the
destruction of laboratory equipment
• Glassvesselsundervacuumwhichcanimplode
• Electriccableswhichcanbedamagedorincorrectlycon-
nected
• Combustiblegasesorsolventvaporsintheareaimmedi-
ately adjacent to the Syncore.
2.6 Warning labels on housing
The following warning sticker(s) can be found on the housing
or assemblies of the Syncore:
Syncore Platform
10
2 Safety
2.7 Safety procedures
The regional and local laws and regulations must be obser-
ved. It is necessary to wear personal protective equipment
such as protective goggles, gloves and a laboratory
coat.
It is only permissible to assemble and dismantle certain parts
of the Syncore when such action is necessary to carry out
the functional requirements.
This activity can be performed manually or by use of the tool
which is supplied. Except for authorized maintenance per-
sonnel, the removal of protective devices and cover plates/
shrouding with the aid of a conventional tool is forbidden.
The owner of the company is responsible for the instruction
of his personnel. To assist in this context, it is possible to
order these Operating Instructions in other languages. At all
times, these Operating Instructions must be available - as a
component part of Syncore - to the operating personnel at
the point where the equipment is employed.
The owner of the company will inform the Manufacturer
immediately regarding all events having a bearing on safety
which take place while the equipment is in use.
2.8 Modifications
No modifications may be made on this unit or on spare and
accessory parts, nor is use of spare or accessory parts other
than those indicated in this Operation Manual permissible,
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