Biotage Selekt Mode d’emploi
© Biotage 2019
Biotage®Selekt PM Checklist | Page
Biotage®Selekt Preventive
Maintenance Checklist
Scope
The tasks carried out during the maintenance visit shall include
servicing the listed components and a final check which is
based on factory acceptance and qualifications tests. These two
procedures constitute a Biotage®Selekt Preventive Maintenance
(PM) Plan.
Each Preventive Maintenance visit should be completed within
two hours (per system) and the system returned to operational
status – unless of course a significant problem is identified.
During the PM visit, the system is disassembled, serviced,
re-assembled and given a performance / function test to help
ensure that it will remain in good working order for the following
year.
Preventive Maintenance is a recommended procedure by
Biotage to reduce the instrument downtime and assure reliable
operation, functionality and accuracy of your Selekt system.
Customer Responsibility
The customer should ensure that the site is prepared in agree-
ment with the guidelines provided in advance.
The checks that follow include the listed configurations
»
SEL-2SV, SEL-2SW, SEL-2EV, SEL-2EW
Items for the Technician to Bring
P/N Description Qty. Notes
Biotage®Selekt use PM kit P/N: 416832SP
416832SP
416424SP, SFÄR-SAMPLET-
TM1, FSUD-0443-0010,
416015SP, 413245SP
1
Grease, test mix
kit, Tube Column
Inlet CPL, FC
needle
Spare Parts to Carry at PM Visit
SFAR-TM1 SFÄR SAMPLE TEST KIT #1 6 Normal Phase
Chomatography
SFAR-TM1-
HMN SFÄR SAMPLE TEST KIT #2 6Reverse Phase
Chomatography
415115SP INLINE CHECK VALVE 4As needed
415950SP ACCESSORY KIT 1As needed
415599SP DEUTERIUM LAMP 1consumbale
416331SP UV CELL, WITH 1/4-28
THREAD 1As needed
416427SP COLUMN HOLDER SFÄR 5G
W. CLIP, 1 PCS. 1As needed
413774 PTFE spray 1Lubrication
416025SP VALVE SOLVENT 1As needed
416026SP VALVE, HIGH PRESSURE 1As needed
UI423 BIOTAGE®SELEKT PM
CHECKLIST 1Copy to carry
Test Tools to Carry at PM Visit
356633SP CALIBRATION KIT 1Pressure test tool
416889SP CALIBRATION ACCESSORY
TOOL KIT 1Pressure test tool
accessory
416411SP CALIBRATION TOOL 1Fraction collector
calibration pin
Customer Information System Information
Company: System Serial#:
Name: System model#:
Email: Date of last PM:
Phone: Estimate date of next PM:
© Biotage 2019
Biotage®Selekt PM Checklist | Page
PrePM Report
√PM Task Notes
Print the System Status and Statistics Report.
The statistic report can be requested prior to the visit. Use the data and run rate
in the report to determine the wear and tear parts and to predict and make pro-
active replacments during the PM.
Clean and Inspect
√PM Task Notes
Open the Selekt door/covers and remove any dust/
debris.
Turn off the system and unplug the power cord from the power source. Pay
particular attention to cooling fans. 3 fans in total plus the power supply fan.
Inspect internal connectors. Check for proper contact and placement.
Clean the display and exterior of the instrument.
Clean the QR code reader. Use a cloth to wipe.
Inspect external and internal tube connections and
ensure all fittings are tight and leak free. Look for leak evidence.
Inspect the solvent inlet filters.
If clogged, advise the customer to use sonication on the filters or how to order
and replace with new. Refer to the user manual and the Maintenance chapter.
Biotage recommendation is to replace filters every 1000 hours run time.
Inspect and test the leak detectors. If applicable.
Pump and Flow Path
System Status and Statistic Report
Valve Status (switches) S1: S2: S3: S4:
Air: BP: Waste:
Pump Strokes Above 20 Bar Strokes:
Pump Board Temp Above 50 °C Minutes:
Controller Board Temp Above 50 °C Minutes:
Pump status
OK Be aware Warning
Comments:
© Biotage 2019
Biotage®Selekt PM Checklist | Page
√PM Task Notes
Lubricate the pump screws. Refer to the Service manual for details and instructions.
Replace the tube (column inlet) Part number 416015SP.
Replace broken capillary holders if worn or broken. Part number 416427SP.
Prime solvents from all channels. Check one at a
time. Verify that no air bubbles are present. If air bubbles are visible check for leaks.
Run a Pump Pressure and Safety Test Record the result. Refer to the Pump pressure and safety test. if the test fails,
replace all four check valves (415115SP).
Perform a Gradient and Pump Performance Test
and record the result.
Fill two volumetric flasks of an equal volume of 100 ml. From the Flush and Purge
menu in the SW, dispense 100 mL at 25 mL/min at a 50:50 ratio between S1 and
S2. Collect the volume to an an empty volumetric flask from C1 or C2. Record the
result.
Gradient equation:
Pump equation:
Fraction Collector
System Status and Statistic Report
Fraction Valve Strokes Number:
X-movment (meters) Distance:
Y-movment (meters) Distance:
Frac status
OK Be aware Warning
Comments:
√PM Task Notes
Check and adjust (if necessary) the level of the
system.
Adjust (elevate) the front legs to assure that the instrument leans backwards to
avoid possible leakage to front.
Check the functionality of the RFID reader. Check all RFID’s by inserting a tray in each position.
Replace the FC needle. 413245 is the standard needle.
Check and verify that the cable moves freely and
without restrictions in all positions.
Pay particular attention to the cable to the FC valve. If the FC valve needs to
be replaced or has been replaced in the past. Make sure the cable is properly
strapped.
Check that the collect valve tubes are not caught
as the arm moves. Adjust if necessary.
(100 – S1) – 0.5
(100 – S1) + (100 – S2)
(C1 or C2 – 100) – 0.5
100
© Biotage 2019
Biotage®Selekt PM Checklist | Page
Check the ribbon cable and verify that it's not
jamming as the arm moves in the Y-direction.
Check the alignment of the X-motor as the arm
moves in the X-direction.
Verify correct belt tension and the FC movement. Adjust if necessary.
Clean and lubricate the arm. Use alcohol to clean the arm and lubricate with 413774 ONLY.
Run a Fraction Function test
Verify in Service mode that all four fraction corner positions (both X and Y position)
are correct and aligned over the proper spot. If needed calibrate using the Selekt
calibration tool. Record the result.
UV Detector
System Status and Statistic Report
Total lamp burn time (h) Time:
Last calibration date Date:
Number of ignitions Counts:
Integration Time (Gain Factor) Time (ms):
UV Detector status
OK Be aware Warning
Comments:
√PM Task Notes
Remove the UV cell and inspect for contamination
or signs of leakage. If the Cell is heavliy contaminated or dirty it will not pass calibration.
Clean the Cell by flushing it with MeOH
Refer to the user manual for cleaning guidance. Ultrasonication may be neccesary.
If the UV cells needs to be replaced advise the customer that a new calibration of
the UV cell is necessary.
Calibrate the UV Detector Record the result. If calibration fails possible causes are dirty or contaminted cell
or faulty/worn UV lamp.
Final Checks
√PM Task Notes
Run the Performance and Verification test as per
UI410, using the test mix in the PM kit. Record the
result.
Record the ratio between peak 1 and peak 2.
© Biotage 2019
Biotage®Selekt PM Checklist | Page
Literature Number: UI423
© 2019 Biotage. All rights reserved. No material may be reproduced or published without the written permission of Biotage.
Information in this document is subject to change without notice and does not represent any commitment from Biotage. E&OE.
A list of all trademarks owned by Biotage AB is available at www.biotage.com/legal. Other product and company names mentioned
herein may be trademarks or registered trademarks and/or service marks of their respective owners, and are used only for
explanation and to the owners’ benefit, without intent to infringe.
Record Section
Gradient Test
Deviation % value
Accepted critera +/- 2%
Pass/Fail Pass Fail
Pump Pressure Test
Pressure Reading Setpoint 1 Pass Fail
Acceptance pressure reading range +/- 1 bar
Pressure Reading Setpoint 2 Pass Fail
Pressure Reading Setpoint 3 Pass Fail
Fraction Collector Function test
Calibration Performed Yes No
Pass/Fail Pass Fail
UV Detector Calibration
Pass/Fail Pass Fail
Pump Volume Test
Deviation % value
Accepted criteria +/- 2%
Pass/Fail Pass Fail
Safety Test
Pass/Fail Pass Fail
Performance and Verification Test
Ratio Accepted criteria 0.84 +/- 0.15
Pass/Fail Pass Fail
Service Review
√PM Task
Review the service and test results with customer.
Record the PM service in a logbook if applicable.
Attach the report from the Checkout test to the PM report.
Attach the compete PM report and statistic report to the the electronic WO (if applicable)
Signatures and System Information
Location:
Biotage Engineer: Date:
Customer: Date:
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