Agilent Technologies InfinityLab LC Series Manuel utilisateur

Agilent InfinityLab LC Series

1260 Infinity II Isocratic and Quaternary Pumps

User Manual

Agilent InfinityLab LC Series 1260 Infinity II Isocratic and Quaternary Pumps User Manual

Notices

Document Information

Document No: SD-29000225 Rev. F

Edition: 07/2023

No part of this manual may be repro-

duced in any form or by any means

(including electronic storage and retrieval

or translation into a foreign language)

without prior agreement and written con-

sent from Agilent Technologies, Inc. as

governed by United States and interna-

tional copyright laws.

Warranty

The material contained in this document

is provided “as is,” and is subject to being

changed, without notice, in future edi-

tions. Further, to the maximum extent

permitted by applicable law, Agilent dis-

claims all warranties, either express or

implied, with regard to this manual and

any information contained herein, includ-

ing but not limited to the implied warran-

ties of merchantability and fitness for a

particular purpose. Agilent shall not be lia-

ble for errors or for incidental or conse-

quential damages in connection with the

furnishing, use, or performance of this

document or of any information con-

tained herein. Should Agilent and the user

have a separate written agreement with

warranty terms covering the material in

this document that conflict with these

terms, the warranty terms in the separate

agreement shall control.

Technology Licenses

The hardware and/or software described

in this document are furnished under a

license and may be used or copied only in

accordance with the terms of such

license.

Restricted Rights Legend

U.S. Government Restricted Rights. Soft-

ware and technical data rights granted to

the federal government include only

those rights customarily provided to end

user customers. Agilent provides this

customary commercial license in Soft-

ware and technical data pursuant to FAR

12.211 (Technical Data) and 12.212

(Computer Software) and, for the Depart-

ment of Defense, DFARS 252.227-7015

(Technical Data - Commercial Items) and

DFARS 227.7202-3 (Rights in Commer-

cial Computer Software or Computer

Software Documentation).

Safety Notices

CAUTION

A CAUTION notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly per-

formed or adhered to, could result

in damage to the product or loss

of important data. Do not proceed

beyond a CAUTION notice until

the indicated conditions are fully

understood and met.

WARNING

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly per-

formed or adhered to, could

result in personal injury or death.

Do not proceed beyond a WARN-

ING notice until the indicated

conditions are fully understood

and met.

Agilent Technologies

Hewlett-Packard-Strasse 8

76337 Waldbronn, Germany

Agilent InfinityLab LC Series 1260 Infinity II Isocratic and Quaternary Pumps User Manual 3

In This Guide...

This manual covers:

•Agilent 1260 Infinity II Isocratic Pump (G7110B),

•Agilent 1260 Infinity II Quaternary Pump VL (G7111A),

•Agilent 1260 Infinity II Quaternary Pump (G7111B), and

•Agilent 1260 Infinity II Bio-inert Pump (G5654A).

1Introduction

This chapter gives an introduction to the module, instrument overview, and internal

connectors.

2 Site Requirements and Specifications

This chapter provides information on environmental requirements, physical, and

performance specifications.

3UsingthePump

This chapter provides information for optimized usage of the module.

4 Optimizing Performance

This chapter gives hints on how to optimize the performance or use additional

devices.

5Troubleshootingand Diagnostics

This chapter gives an overview about the troubleshooting and diagnostic features

and the different user interfaces.

6 Error Information

This chapter describes the meaning of error messages, and provides information

on probable causes and suggested actions how to recover from error conditions.

Agilent InfinityLab LC Series 1260 Infinity II Isocratic and Quaternary Pumps User Manual 4

7 Test Functions and Calibration

This chapter describes the tests for the module.

8 Maintenance

This chapter describes the maintenance of the module.

9 Parts for Maintenance

This chapter provides information on parts for maintenance.

10 Identifying Cables

This chapter provides information on cables used with the Agilent 1200 Infinity

Series modules.

11 Hardware Information

This chapter describes the pump in more detail on hardware and electronics.

12 LAN Configuration

This chapter provides information on connecting the module to the Agilent

ChemStation PC.

13 Appendix

This chapter provides addition information on safety, legal, and web.

Agilent InfinityLab LC Series 1260 Infinity II Isocratic and Quaternary Pumps User Manual 5

Contents

1Introduction9

Introduction to the Pump 10

G7110B Isocratic Pump 11

G7111A Quaternary Pump VL 13

G7111B Quaternary Pump 15

G5654A Bio-inert Pump 17

Overview of the Hydraulic Path 19

Leak and Waste Handling 26

2 Site Requirements and Specifications 31

Site Requirements 32

Physical Specifications 35

Performance Specifications 39

3UsingthePump46

Magnets 47

Turn on/off 48

Status Indicators 50

Best Practices 51

Leak and Waste Handling 53

Hints for Successful Use of the Pump 55

Setting up the Pump with the G4208A Instant Pilot 56

Setting up the Pump with the Instrument Control Interface 57

Solvent Information 65

Algae Growth in HPLC Systems 74

Prevent Blocking of Solvent Filters 75

Normal Phase Applications 76

Agilent InfinityLab LC Series 1260 Infinity II Isocratic and Quaternary Pumps User Manual 6

4 Optimizing Performance 78

Using the Degasser 79

Operational Hints for the Vacuum Degasser 80

Operational Hints for the Multi Channel Gradient Valve (MCGV) 81

When to use the Seal Wash Function 82

Choosing the Right Pump Seals 83

Optimize the Compressibility Compensation Setting 84

5 Troubleshooting and Diagnostics 86

User Interfaces 87

Agilent Lab Advisor Software 88

6 Error Information 89

What Are Error Messages 90

General Error Messages 91

Module Error Messages 99

7 Test Functions and Calibration 111

Introduction 112

System Pressure Test 113

Leak Rate Test 118

8 Maintenance 124

Introduction to Maintenance and Repair 125

Warnings and Cautions 126

Overview of Maintenance and Repair 127

Cleaning the Module 128

Remove and Install Doors 129

Checking and Replacing the Solvent Filter 131

Exchange the Passive Inlet Valve 132

Exchange the Outlet Valve 134

Exchange the Purge Valve Frit or the Purge Valve 136

Replace the O-Ring on the Purge Valve 139

Remove the Pump Head Assembly 141

Agilent InfinityLab LC Series 1260 Infinity II Isocratic and Quaternary Pumps User Manual 7

Maintenance of a Pump Head Without Seal Wash Option 143

Maintenance of a Pump Head with Seal Wash Option 146

Reinstall the Pump Head Assembly 151

Seal Wear-in Procedure 154

Exchange the Multi-Channel Gradient Valve (MCGV) 155

Replace the Solvent Selection Valve (Isocratic Pump) 158

Exchange the Active Inlet Valve (AIV) or its Cartridge 160

Exchange the Seal Wash Cartridge 162

Replace Leak Handling System Parts 163

Replacing the Module Firmware 164

9 Parts for Maintenance 165

Accessory Kits 166

Pump Head Assembly Without Seal Wash 168

Pump Head Assembly with Seal Wash Option 170

Outlet Valve 173

Purge Valve Assembly 174

Active Inlet Valve Assembly 175

1260 Infinity II Max Uptime Kit 177

1260 Infinity II Max Uptime Kit Bio 178

1260 Infinity II Low Dispersion Kit MCT 179

HPLC System Tool Kit 180

Solvent Cabinet 181

Bottle Head Assembly 182

Hydraulic Path of the Quaternary Pump 183

Hydraulic Path of the Isocratic Pump 185

10 Identifying Cables 186

Cable Overview 187

Analog Cables 189

Remote Cables 191

CAN Cable 195

Agilent Module to PC 196

Agilent 1200 Module to Printer 197

Agilent InfinityLab LC Series 1260 Infinity II Isocratic and Quaternary Pumps User Manual 8

11 Hardware Information 198

Firmware Description 199

Electrical Connections 202

Interfaces 204

Setting the 6-bit Configuration Switch 212

Instrument Layout 216

Early Maintenance Feedback 217

12 LAN Configuration 218

What You Have to Do First 219

TCP/IP parameter configuration 220

Configuration Switches 221

Initialization Mode Selection 222

Dynamic Host Configuration Protocol (DHCP) 224

Manual Configuration 227

13 Appendix 232

General Safety Information 233

Waste Electrical and Electronic Equipment (WEEE) Directive 239

Radio Interference 240

Sound Emission 241

Agilent Technologies on Internet 242

Agilent InfinityLab LC Series 1260 Infinity II Isocratic and Quaternary Pumps User Manual 9

1Introduction

Introduction to the Pump 10

G7110B Isocratic Pump 11

Product Description 11

Features 12

G7111A Quaternary Pump VL 13

Product Description 13

Features 14

G7111B Quaternary Pump 15

Product Description 15

Features 16

G5654A Bio-inert Pump 17

Product Description 17

Features 18

Overview of the Hydraulic Path 19

Hydraulic Path 20

How Does the Pump Work? 22

How Does Compressibility Compensation Work? 25

How Does Variable Stroke Volume Work? 25

Leak and Waste Handling 26

Leak Sensor 29

Waste Concept 30

This chapter gives an introduction to the module, instrument overview, and

internal connectors.

1Introduction

Introduction to the Pump

Agilent InfinityLab LC Series 1260 Infinity II Isocratic and Quaternary Pumps User Manual 10

Introduction to the Pump

The Pumps comprise one pump head unit with an optional solvent cabinet, a

vacuum degasser (optional for the isocratic pump), and a multi-channel gradient

valve (MCGV) for quaternary pumps, or an optional solvent selection valve (SSV)

for isocratic pumps. The combination of the pump head assembly and

high-speed proportioning MCGV with a possible connection up to four different

solvents in quaternary pumps provides gradient generation by low pressure

mixing. The combination of the pump head assembly and SSV in isocratic pump

provides opportunity to make a choice between three different solvents. A

solvent cabinet provides enough space for eight one-liter bottles. The Active Seal

Wash (ASW) and Active Inlet Valve (AIV) options are available for quaternary

pumps when concentrated buffer solutions are used. The Bio-inert pump is

optimized for these conditions, thus is always equipped with ASW and AIV.

Figure 1 Overview of the pump

Degasser

MCGV

Inlet Valve

Outlet Valve

Pump Head

Purge Valve

Autres manuels pour InfinityLab LC Series

Ce manuel convient aux modèles suivants

Table des matières

Autres manuels Agilent Technologies Pompe à eau

Agilent Technologies

Agilent Technologies TwisTorr 304 FS Manuel utilisateur

Agilent Technologies

Agilent Technologies 1200 series Manuel utilisateur

Agilent Technologies

Agilent Technologies TV 301SF Navigator Manuel utilisateur

Agilent Technologies

Agilent Technologies 1290 Infinity II Manuel utilisateur

Agilent Technologies

Agilent Technologies IDP-15 Guide de référence

Agilent Technologies

Agilent Technologies G6696A Manuel utilisateur

Agilent Technologies

Agilent Technologies TriScroll 800 Manuel utilisateur

Agilent Technologies

Agilent Technologies MS120 Manuel utilisateur

Agilent Technologies

Agilent Technologies 1260 Infinity Manuel utilisateur

Agilent Technologies

Agilent Technologies 1260 Infinity II Manuel utilisateur

Agilent Technologies

Agilent Technologies IDP 10 Manuel utilisateur

Agilent Technologies

Agilent Technologies HS-16 Manuel utilisateur

Agilent Technologies

Agilent Technologies 1260 Infinity II Manuel utilisateur

Agilent Technologies

Agilent Technologies X3502-64170 Manuel utilisateur

Agilent Technologies

Agilent Technologies IDP-15 Manuel utilisateur

Agilent Technologies

Agilent Technologies TriScroll 800 Manuel utilisateur

Agilent Technologies

Agilent Technologies HS452 Manuel utilisateur

Agilent Technologies

Agilent Technologies Turbo-V 1K-G Series Manuel utilisateur

Agilent Technologies

Agilent Technologies TriScroll 300 Series Manuel d'utilisation et d'entretien

Agilent Technologies

Agilent Technologies 1100 Series Manuel utilisateur

Agilent Technologies

Agilent Technologies G6697A IDP-10 Manuel utilisateur

Agilent Technologies

Agilent Technologies Turbo-V 1K-G Series Manuel utilisateur

Agilent Technologies

Agilent Technologies TV-401/301/21 NSF Manuel utilisateur

Agilent Technologies

Agilent Technologies TriScroll 610 Manuel utilisateur

Manuels Pompe à eau populaires d'autres marques

Neptun

Neptun NPHW 5500 Manuel utilisateur

Sensidyne

Sensidyne Gilian BDX-II Instructions d'installation et d'utilisation

Draper

Draper 47808 Manuel utilisateur

Trolla

Trolla 12820 Manuel utilisateur

Sunfab

Sunfab SVH Series Manuel utilisateur

WilTec

WilTec 50740 Manuel utilisateur

Fieldmann

Fieldmann FVC 5015 EK Manuel utilisateur

Everbilt

Everbilt EFSUB5-122HD Manuel utilisateur

Graco

Graco Husky 3300e Manuel utilisateur

esotec

esotec 101018 Manuel utilisateur

moyno

moyno 2000 CC Manuel utilisateur

Becker

Becker BASIC VASF 2.80/1-0.AC230 Manuel utilisateur

Sykes AmeriPumps

Sykes AmeriPumps GP100M Guide de dépannage

DUROMAX

DUROMAX XP WX Series Manuel utilisateur

BRINKMANN PUMPS

BRINKMANN PUMPS SBF550 Manuel utilisateur

Franklin Electric

Franklin Electric IPS Manuel utilisateur

Xylem

Xylem e-1532 Series Manuel utilisateur

Milton Roy

Milton Roy PRIMEROYAL Manuel utilisateur