Agilent Technologies 7890B Manuel d'installation

Agilent Technologies

Agilent 7890B Gas

Chromatograph

Installation and First Startup

Notices

No part of this manual may be reproduced

in any form or by any means (including

electronic storage and retrieval or

translation into a foreign language)

without prior agreement and written

consent from Agilent Technologies, Inc. as

governed by United States and

international copyright laws.

Manual Part Number

G3430-90056

Edition

Third edition, October 2015

Second edition, December 2013 

First edition, January 2013

Printed in USA

Agilent Technologies, Inc.

2850 Centerville Road

Wilmington, DE 19808-1610 USA

安捷伦科技（上海）有限公司

上海市浦东新区外高桥保税区

英伦路 412 号

联系电话：（800）820 3278

Warranty

The material contained in this document is

provided “as is,” and is subject to being

changed, without notice, in future editions.

Further, to the maximum extent permitted

by applicable law, Agilent disclaims all

warranties, either express or implied, with

regard to this manual and any information

contained herein, including but not limited

to the implied warranties of

merchantability and fitness for a particular

purpose. Agilent shall not be liable for

errors or for incidental or consequential

damages in connection with the

furnishing, use, or performance of this

document or of any information contained

herein. Should Agilent and the user have a

separate written agreement with warranty

terms covering the material in this

document that conflict with these terms,

the warranty terms in the separate

agreement shall control.

Safety Notices

WARNING

A WARNING notice denotes a hazard.

It calls attention to an operating

procedure, practice, or the like that, if

not correctly performed or adhered

to, could result in personal injury or

death. Do not proceed beyond a

WARNING notice until the indicated

conditions are fully understood and

met.

CAUTION

A CAUTION notice denotes a hazard.

It calls attention to an operating

procedure, practice, or the like that, if

not correctly performed or adhered to,

could result in damage to the product

or loss of important data. Do not

proceed beyond a CAUTION notice

until the indicated conditions are fully

understood and met.

Agilent 7890B Installation 3

Contents

1 Installing the GC

Overview of Installation 8

Purpose of this procedure 8

Customer responsibilities 8

About Agilent’s installation service 8

Tools and additional parts required 9

Performing checkout 9

System installation 9

The 7890B GC 11

Unpacking 12

Step 1. Place the GC on the bench 13

Step 2. Verify line voltage, voltage settings, and power cord. 14

Power consumption 14

Power cords available 15

Grounding 19

Line voltage 19

Line power cord terminations 19

Step 3. Connect the power cord and turn on the GC 20

Step 4. Connect gases and traps 22

Install the gas regulators 22

Connect the tubing to the gas source 24

Install traps 25

Supplied fittings 26

Plumb to EPC flow modules 26

Install Aux EPC module frits for your application 30

Install hydrogen sensor calibration gas 31

Step 5. Leak test all connections and set source pressures 33

Set source gas pressures 35

Step 6. Vent µECD or uncombusted hydrogen to a fume hood 36

Step 7. Connect cryogenic cooling (if present) 37

Connecting liquid carbon dioxide 38

Connecting liquid nitrogen 40

Connecting air to the multimode inlet 41

Step 8. Connect valve actuator air (if present) 42

Step 9. Install inlet checkout parts 43

Step 10. Install ALS, if ordered 44

4Agilent 7890B Installation

Step 11. Connect the external cables 45

Back panel connectors 45

Connecting cables 48

Labeling BCD and EVENT cables 50

Configuring the GC IP address 50

GC / MS / Agilent data system / ALS 52

Additional cabling configurations 52

Step 12. Finish configuring communications 53

Configuring GC-MS communications (5977A, 7000C, 7010) 53

Configuring GC-MS communications (5877B) 56

Configuring GC-HS communications 56

Step 13. Calibrate the Hydrogen Sensor 58

Step 14. Configure the date/time, pressure units, and the checkout

column 59

Date and time 59

Pressure units 59

Checkout column 59

Step 15. Install the checkout column to the inlet and condition 61

Step 16. Bakeout the detector 63

Step 17. Cool the detector and complete column installation 64

Step 18. If appropriate, update firmware 65

GC firmware 65

PIDs 66

Step 19. Transfer the checkout sample to a screw-top sample vial 67

Step 20. When the system stabilizes, run one injection 68

Step 21. Evaluate Results 69

Prepare for the Next Analysis 70

A Making Swagelok Connections

Making Swagelok Connections 72

Using a Swagelok Tee 75

Agilent 7890B Installation 5

B Cabling Diagrams and Remote Start/Stop

Using the Remote Start/Stop Cable 78

Connecting Agilent products 78

Connecting non-Agilent products 78

Multi-instrument Cabling Examples 81

GC / ALS / Non-Agilent Data System 81

GC / 3395A/3396B Integrator / ALS 82

GC / 3396C Integrator / ALS 83

Example: Using a Y-Cable in a setup (GC/MSD/Data System/Headspace

Sampler) 84

GC / External Events (unspecified, non-Agilent instrument) 85

Cable Diagrams 86

Analog signal cable, general use, G1530-60560 86

Agilent analog signal cable, G1530-60570 87

Remote start/stop cable, general use, 35900-60670 87

Agilent APG remote start/stop cable, 03396-61010 88

Agilent APG remote start/stop cable, G1530-60930 89

Agilent remote start/stop Y-cable, G1530-61200 89

BCD cable, G1530-60590 90

BCD cable, G1530-61100 91

External event cable, G1530-60590 92

External valve cable, G1580-60710 93

Pulser module power supply cable, G1580-60730 94

6Agilent 7890B Installation

Agilent 7890B Gas Chromatograph

Installation and First Startup

Agilent Technologies

Installing the GC

Overview of Installation 8

The 7890B GC 11

Unpacking 12

Step 1. Place the GC on the bench 13

Step 2. Verify line voltage, voltage settings, and power cord. 14

Step 3. Connect the power cord and turn on the GC 20

Step 4. Connect gases and traps 22

Step 5. Leak test all connections and set source pressures 33

Step 6. Vent µECD or uncombusted hydrogen to a fume hood 36

Step 7. Connect cryogenic cooling (if present) 37

Step 8. Connect valve actuator air (if present) 42

Step 9. Install inlet checkout parts 43

Step 10. Install ALS, if ordered 44

Step 11. Connect the external cables 45

Step 12. Finish configuring communications 53

Step 13. Calibrate the Hydrogen Sensor 58

Step 14. Configure the date/time, pressure units, and the checkout

column 59

Step 15. Install the checkout column to the inlet and condition 61

Step 16. Bakeout the detector 63

Step 17. Cool the detector and complete column installation 64

Step 18. If appropriate, update firmware 65

Step 19. Transfer the checkout sample to a screw-top sample vial 67

Step 20. When the system stabilizes, run one injection 68

Step 21. Evaluate Results 69

Prepare for the Next Analysis 70

This section contains installation procedures for the Agilent

7890B GC. Depending on the ordered options, some steps are

optional, such as plumbing cryogenic cooling or valve actuator

air.

Instructions for connecting cables from the GC to other

instruments in a typical 7890 Series system are included here

and in Appendix B, “Cabling Diagrams and Remote Start/Stop."

8Agilent 7890B Installation

1Installing the GC

Overview of Installation

Purpose of this procedure

This procedure ensures that instruments and systems are

installed and functioning as designed. Correct installation is the

first step in ensuring that instruments and systems operate

reliably over their lifetime.

Customer responsibilities

1Make sure your site meets the basic requirements, including

the necessary space, electrical outlets, gases, tubing,

operating supplies, consumables and other usage-dependent

items required for a successful installation. Refer to the

Agilent GC, GC/MS, and ALS Site Preparation Guide.

2If Agilent is delivering installation and familiarization

services, users of the instrument should be present

throughout these services; otherwise, these users will miss

important operational, maintenance, and safety information.

Additional information is included with the Agilent GC and

GC/MS User Manuals & Tools DVD.

If your site complies with all site preparation specifications, the

average installation time for the GC is about 2 hours. Allow

more time for any additional products (for example, an ALS),

add-ons, and software.

About Agilent’s installation service

The installation service does not include:

•Network setup with other computers or to the site or

building LAN.

•Customization of the system.

•Method development and testing.

•Analysis of customer standards or samples.

•Testing against the instrument performance specification.

(Operational qualification and performance verification

services, OQ/PV, can be purchased separately.)

If you need assistance beyond this installation service, please

contact your local Agilent Technologies office. Assistance with

installation and with user-specific services and applications is

available and will be contracted separately.

Installing the GC 1

Agilent 7890B Installation 9

Tools and additional parts required

Installation requires the following tools, fittings, and hardware.

These items are not included with the instrument.

•Precleaned copper tubing, 1/8-inch or 1/4-inch od.

•Fittings.

•Tubing cutter.

•Filters for gas supplies.

•7/16-inch and 9/16-inch wrenches for assembling Swagelok

fittings.

•Carrier and other gas supplies.

•Pressure regulator for each gas supply.

•A computer with a LAN connection (for reading GC

documentation and for updating GC firmware if needed).

•Any additional LAN components, such as cables and a switch

or hub, for connection to the site LAN (not included in

Agilent installation services).

The Agilent GC, GC/MS, and ALS Site Preparation Guide

contains a listing of Agilent installation kits and a description of

parts included with each. These kits contain filters, fittings,

tubing, tools (wrenches, tubing cutter, drivers, and so on), and

other required parts for installing a GC.)

Performing checkout

Checkout requires a system that can produce a chromatogram.

•If using an Agilent data system, you can use it to perform the

checkout procedure. Read these GC installation instructions

and the instructions for installing the data system.

•If an Agilent data system is not available, you can also

perform checkout using the Agilent Instrument Utilities

software. Install the software on a PC, then read its help

topics to learn how to connect to the GC and how to launch

the checkout procedures.

•If connected only to an integrator or site system (for

example, a LIMS system) that captures the GC output signal,

you must connect to that system to obtain the

chromatogram.

System installation

If installing an ALS, the ALS can be used for checkout. Also

10 Agilent 7890B Installation

1Installing the GC

refer to the ALS installation documentation.

When installed as part of a complete system including an

Agilent data system (for example, Agilent OpenLAB CDS), first

install the GC through the checkout column bakeout step. Once

the bakeout ends, configure the new GC in the data system and

open the online instrument session. Use the data system to

perform the checkout test.

When installed as part of other complete systems, for example

in an Agilent GC/MSD or GC/MS system, see the installation

instructions for that system.

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