Teledyne 6200A Manuel utilisateur

MODEL 6200A

TRS ANALYZER

MANUAL ADDENDUM

TELEDYNE ANALYTICAL INSTRUMENTS

03655 Rev. A, August, 2000

TAI - Thermal Converter Operator Manual - Page i

TABLE OF CONTENTS

TABLE OF CONTENTS ..............................................................................................I

TABLE OF FIGURES...................................................................................................I

1.0 WARRANTY............................................................................................................1

1.1 Claims for damaged shipments..................................................................................2

1.2 Claims for shipping discrepancies .............................................................................2

2.0 INTRODUCTION....................................................................................................3

2.1 Specifications.............................................................................................................3

2.1.1 Analyzer Specifications ..................................................................................3

2.1.2 TRS Converter Specifications.........................................................................3

2.2 The Sulfides Analyzer...............................................................................................4

2.3 Configurations............................................................................................................4

2.4 The TRS – Total Reduced Sulfur Converter..............................................................8

2.5 Installation..................................................................................................................10

2.6 Operation and Calibration..........................................................................................12

2.6.1 Calibration Theory..........................................................................................12

2.6.2 Zero and Span Calibration Procedure.............................................................13

2.7 M501TRS Temperature Controller............................................................................14

2.7.1 Changing the Temperature Set Point ..............................................................14

2.7.2 Adjusting the P-I-D Parameters......................................................................15

3.0 TROUBLESHOOTNG............................................................................................17

4.0 MAINTENANCE.....................................................................................................19

4.1 SO2 Analyzer Maintenance .......................................................................................19

4.2 Changing the Quartz Tube.........................................................................................19

4.3 Checking the Converter Efficiency............................................................................19

4.4 Sample Diluter Maintenance......................................................................................20

TAI - Thermal Converter Operator Manual - Page i

TABLE OF FIGURES

FIGURE 2.1 – STANDARD CONFIGURATION 5

FIGURE 2.2 – WITH IZS OPTION 6

FIGURE 2.3 – WITH M702 CALIBRATOR OPTION 7

FIGURE 2.4 – TRS CONVERTER LAYOUT 9

FIGURE 2.5 – PNEUMATIC CONNECTIONS 11

FIGURE 3.1 – TRS WIRING DIAGRAM 18

FIGURE 4.1 – DILUTER FLOW BLOCK ASSEMBLY 21

TAI - Thermal Converter Operator Manual - Page i

TABLE OF TABLES

TABLE 2.1 – TRS CONVERTER SPECIFICATIONS.............................................................................................................3

TABLE 2.2 – ZERO CALIBRATION PROCEDURE..............................................................................................................13

TABLE 2.3 – SPAN CALIBRATION PROCEDURE..............................................................................................................14

TABLE 2.4 – TEMPERATURE CONTROLLER - INITIAL SETTINGS...............................................................................16

TABLE 2.5 – TEMPERATURE CONTROLLER - SECONDARY MENU ............................................................................16

TAI - Thermal Converter Operator Manual - Page 1

1.0 WARRANTY

TELEDYNE ANALYTICAL INSTRUMENTS

02024c

Prior to shipment, TAI equipment is thoroughly inspected and tested. Should equipment failure occur, TAI

assures its customers that prompt service and support will be available.

COVERAGE

After the warranty period and throughout the equipment lifetime, TAI stands ready to provide on-site or in-

plant service at reasonable rates similar to those of other manufacturers in the industry. All maintenance

and the first level of field troubleshooting are to be performed by the customer.

GENERAL

TAI warrants each Product manufactured by TAI to be free from defects in material and workmanship under

normal use and service for a period of one year from the date of delivery. All replacement parts and repairs

are warranted for 90 days after the purchase.

If a Product fails to conform to its specifications within the warranty period, TAI shall correct such defect

by, in TAI's discretion, repairing or replacing such defective Product or refunding the purchase price of such

Product.

The warranties set forth in this section shall be of no force or effect with respect to any Product:

(i) that has been altered or subjected to misuse, negligence or accident, or (ii) that has been used in any

manner other than in accordance with the instruction provided by TAI or (iii) not properly maintained.

THE WARRANTIES SET FORTH IN THIS SECTION AND THE REMEDIES THEREFORE ARE

EXCLUSIVE AND IN LIEU OF ANY IMPLIED WARRANTIES OF MERCHANTABILITY, FITNESS

FOR PARTICULAR PURPOSE OR OTHER WARRANTY OF QUALITY, WHETHER EXPRESSED

OR IMPLIED. THE REMEDIES SET FORTH IN THIS SECTION ARE THE EXCLUSIVE REMEDIES

FOR BREACH OF ANY WARRANTY CONTAINED HEREIN. TAI SHALL NOT BE LIABLE FOR

ANY INCIDENTAL OR CONSEQUENTIAL DAMAGES ARISING OUT OF OR RELATED TO THIS

AGREEMENT OF TAI'S PERFORMANCE HEREUNDER, WHETHER FOR BREACH OF

WARRANTY OR OTHERWISE.

TERMS AND CONDITIONS

All units or components returned to TAI should be properly packed for handling and returned

freight prepaid to the nearest designated Service Center. After the repair, the equipment will be

returned, freight prepaid.

TAI - Thermal Converter Operator Manual - Page 2

1.1 Claims for damaged shipments

All instruments should be thoroughly inspected immediately upon receipt. Material in the container

should be checked against the enclosed packing list. If the contents are damaged and/or the instrument

fails to operate properly, the carrier and TAI should be notified immediately.

The following documents are necessary to support claims:

•Original freight bill and bill of lading

•Original invoices or photocopy of original invoice

•Copy of the packing list

•Photographs of damaged equipment and container

1.2 Claims for shipping discrepancies

All containers should be checked against packing list immediately upon receipt. If a shortage occurs,

notify the carrier and TAI immediately. TAI will not be responsible for shortages against the packing list

unless they are reported immediately.

The following information is necessary to make a claim:

•The instrument model number

•Serial number

•Sales order number or purchase order number

Upon receipt of a claim, TAI will advise disposition of the equipment for repair or replacement.

TAI - Thermal Converter Operator Manual - Page 3

2.0 INTRODUCTION

This manual addendum should be used in conjunction with the standard Model 6200A.

2.1 Specifications

2.1.1 Analyzer Specifications

The specifications for the SO2 analyzer are contained in the standard Model 6200A manual.

2.1.2 M501TRS Converter Specifications

TABLE 2.1 – M501TRS Converter Specifications

Specification Value Unit

Flow Rate 1000 Cc/min maximum

TRS Concentration 20 ppm

Converter Temperature 950 – 1050 oC

Dilution Ratio 4.3:1 Number

Conversion Eff. (H2S) >98 %

Power 220 VAC, 50/60 Hz, 220 watts

Weight 24 lbs

11 kg

Dimensions 7 x 17 x 22 inches

178 x 432 x 559 mm

TAI - Thermal Converter Operator Manual - Page 4

2.2 The 6200A Sulfides Analyzer

The TAI Model 6200A Sulfides Analyzer, is designed to measure mixed sulfur impurities, collectively

referred to as TRS, in carbon dioxide (CO2) gas. Since there is no SO2 scrubber in the system, the

instrument reading is the sum of the reduced sulfur compounds and SO2. The 6200A consists of a

modified 6200A UV Fluorescence SO2Analyzer and a M501TRS high temperature quartz converter.

The M501TRS converts sulfur compounds to SO2at high temperature by flowing the gas through a hot

quartz tube, the resultant reaction is as follows:

TRS + O2--> SO2

Since the gas being analyzed is CO2, which generally contains no oxygen, there is an assembly that injects

a small amount of air into the sample stream resulting in about 4% oxygen in the sample. The added

oxygen allows the sulfur compounds to be oxidized to SO2. Any SO2 present in the sample is unaffected

by the converter. The sample gas then passes to a modified 6200A analyzer where the converted

compounds are analyzed as SO2.

2.3 Configurations

There are three configurations available:

1. The standard unit consisting of:

•A modified 6200A Fluorescent SO2 Analyzer

•A M501TRS High Temperature Converter

•See Figure 2.1 for the pneumatic diagram

2. The standard unit described above plus:

•An Internal Zero/Span (IZS) Option with H2S permeation tube

•The IZS option uses sample gas, passed through a charcoal scrubber to dilute H2S from

the perm tube plus a converter bypass valve to assure a high quality zero/span

calibration.

•See Figure 2.2 for the pneumatic diagram

3. The standard unit described above plus:

•An external PRC-6000 calibrator for blending tanks of H2S or SO2 span gas with CO2.

•See Figure 2.3 for the pneumatic diagram

TAI - Thermal Converter Operator Manual - Page 5

FIGURE 2.1 – BASIC CONFIGURATION

TAI - Thermal Converter Operator Manual - Page 6

FIGURE 2.2 – WITH IZS OPTION

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