Metrohm 815 Manuel utilisateur

815 Robotic Soliprep for LC

2.815.4110

Manual

8.815.8002EN / 2020-02-29

Metrohm AG

CH-9100 Herisau

Switzerland

Phone +41 71 353 85 85

Fax +41 71 353 89 01

[email protected]

www.metrohm.com

815 Robotic Soliprep for LC

2.815.4110

Manual

8.815.8002EN / 2020-02-29

Technical Communication

Metrohm AG

CH-9100 Herisau

[email protected]

This documentation has been prepared with great care. However, errors

can never be entirely ruled out. Please send comments regarding possible

errors to the address above.

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Table of contents

815 Robotic Soliprep for LC ￭￭￭￭￭￭￭￭ III

Table of contents

1 Introduction 1

1.1 Instrument description ......................................................... 1

1.2 Intended use ......................................................................... 2

1.3 About the documentation ................................................... 2

1.3.1 Symbols and conventions ........................................................ 2

1.4 Safety instructions ................................................................ 3

1.4.1 General notes on safety ........................................................... 3

1.4.2 Electrical safety ........................................................................ 3

1.4.3 Personnel safety ....................................................................... 4

1.5 Recycling and disposal ......................................................... 5

2 Installation 6

2.1 Preparing the Sample Processor ......................................... 6

2.2 Connecting the instrument to the power grid ................... 8

2.3 Installing MagIC Net™ ......................................................... 9

2.4 Configuring the Swing Heads .............................................. 9

2.5 Mounting the Swing Heads ............................................... 13

2.6 Mounting the deflector, Luer connector and collection

container ............................................................................. 16

2.7 Mounting the transfer robotic arm ................................... 20

2.8 Mounting the Polytron robotic arm .................................. 24

2.9 Washing station and drip pan ........................................... 25

2.10 Connecting and setting up the peristaltic pump ............. 27

2.11 Installing the rinsing tubing .............................................. 29

2.12 Placing tubing and cables in the guide chain .................. 29

2.13 Assembling and mounting the Polytron® drive ................ 31

2.14 Mounting the rinsing tubings for the Polytron® ............. 31

2.15 Connecting the Polytron® .................................................. 32

2.16 Mounting the safety shield ................................................ 33

2.17 Installing the Dosino .......................................................... 34

2.18 Equipping the rack ............................................................. 37

3 Defining rack positions 39

4 Adjusting rack and robotic arm 41

Table of contents ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

IV ￭￭￭￭￭￭￭￭ 815 Robotic Soliprep for LC

5 Setting lift positions 45

5.1 Lift position for sample beakers ....................................... 45

5.2 Lift position for picking up needles and filters ................ 46

5.3 Lift positions for special beakers ...................................... 47

5.4 Lift positions for stripping needles and filters ................. 49

5.5 Lift position for the Luer connector .................................. 51

5.6 Lift position for the Polytron ............................................. 52

5.7 Lift position for the washing station ................................ 53

6 Controlling the Polytron® 55

7 Accessories 60

Index 61

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 1 Introduction

815 Robotic Soliprep for LC ￭￭￭￭￭￭￭￭ 1

1 Introduction

1.1 Instrument description

The 815 Robotic Soliprep systems are automation systems suitable for a

variety of uses. They have been designed exclusively for utilization in facto-

ries and laboratories and cover a wide range of applications. Soliprep sys-

tems can be used for automation purposes wherever a complex sample

preparation of solid substances is required, e.g. for pharmaceutical or food

analysis.

The Robotic Sample Processors, which have proven their worth for many

years, form the basis for a versatile system that has been expanded to

include opportunities for the dispersion, filtration and bottling of samples

of all sorts. This versatile concept can be expanded as required.

Thanks to the integration of high-performance communication interfaces

(USB, RS-232), they can be incorporated seamlessly into a variety of instru-

ment systems, and not only those manufactured by Metrohm. Operation

by the high performance tiamo™ or MagIC Net™ software ensures not

only user-friendly operation and programming of automation sequences,

but also allows 100% conformity for the entire automation system with

FDA (Food and Drug Administration) regulations. This applies in particular

with regard to regulation 21 CFR Part 11, Electronic records and signa-

tures.

815 Robotic Soliprep for Liquid Chromatography

￭Dispersion, filtration, dilution and sample transfer

The universal automation system for sample preparation in instrumental

chromatography. A workstation equipped with a dispersion device is used

to shred the sample. The dispersion aggregate is cleaned in a special rins-

ing station. The second workstation is equipped for sample transfer with a

universal robotic arm with a Luer adapter. It is used for picking up syringe

needles (for aspirating the dispersed sample and bottling the filtrate in

sealed vials) and membrane filters (for filtering and injecting the sample in

a capillary).

Needles and filters are charged in replaceable inserts. The needles and fil-

ters are automatically stripped off after use and disposed of in a waste

container.

Two versatile dosing drives (800 Dosino) are used as an auxiliary device for

diluting the sample and for transferring the sample solution.

1.2 Intended use ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

2￭￭￭￭￭￭￭￭ 815 Robotic Soliprep for LC

1.2 Intended use

The 815 Robotic Soliprep for LC is designed for the automatic analysis of

larger-sized sample series in analytical laboratories. The functioning of the

automation system comprises crushing, homogenizing and dissolving of

solid samples as well as filtering and transferring the resulting sample solu-

tions. Its main area of application is the sample preparation in instrumen-

tal chromatography. It is not suitable for usage in biochemical, biological

or medical environments in its basic equipment version.

This instrument is suitable for processing chemicals and flammable sam-

ples. Therefore, the use of the 815 Robotic Soliprep for LC requires the

user to have basic knowledge and experience in handling toxic and caustic

substances. Knowledge regarding the application of fire prevention meas-

ures prescribed for laboratories is also mandatory.

1.3 About the documentation

1.3.1 Symbols and conventions

The following symbols and formatting may appear in this documentation:

Cross-reference to figure legend

The first number refers to the figure number, the sec-

ond to the instrument part in the figure.

Instruction step

Carry out these steps in the sequence shown.

Method Dialog text, parameter in the software

File ▶ New Menu or menu item

[Next] Button or key

WARNING

This symbol draws attention to a possible life-threat-

ening hazard or risk of injury.

WARNING

This symbol draws attention to a possible hazard due

to electrical current.

WARNING

This symbol draws attention to a possible hazard due

to heat or hot instrument parts.

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 1 Introduction

815 Robotic Soliprep for LC ￭￭￭￭￭￭￭￭ 3

WARNING

This symbol draws attention to a possible biological

hazard.

CAUTION

This symbol draws attention to possible damage to

instruments or instrument parts.

NOTE

This symbol highlights additional information and

tips.

1.4 Safety instructions

1.4.1 General notes on safety

WARNING

Operate this instrument only according to the information contained in

this documentation.

This instrument left the factory in a flawless state in terms of technical

safety. To maintain this state and ensure non-hazardous operation of the

instrument, the following instructions must be observed carefully.

1.4.2 Electrical safety

The electrical safety when working with the instrument is ensured as part

of the international standard IEC 61010.

WARNING

Only personnel qualified by Metrohm are authorized to carry out service

work on electronic components.

WARNING

Never open the housing of the instrument. The instrument could be

damaged by this. There is also a risk of serious injury if live components

are touched.

There are no parts inside the housing which can be serviced or replaced

by the user.

1.4 Safety instructions ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

4￭￭￭￭￭￭￭￭ 815 Robotic Soliprep for LC

Supply voltage

WARNING

An incorrect supply voltage can damage the instrument.

Only operate this instrument with a supply voltage specified for it (see

rear panel of the instrument).

Protection against electrostatic charges

WARNING

Electronic components are sensitive to electrostatic charges and can be

destroyed by discharges.

Do not fail to pull the power cord out of the power socket before you

set up or disconnect electrical plug connections at the rear of the

instrument.

1.4.3 Personnel safety

WARNING

Personnel are not permitted to reach into the working area of a Sample

Processor while operations are running!

A considerable risk of injury exists for users who undertake manual

interventions to the automatic running of the instrument.

The various drives in a Sample Processor (including Swing Heads) have

considerable power in order to ensure that they are able to be operated

perfectly, even with greater loads. They are equipped with an electronic

overload protection that is activated in the presence of excessive mechani-

cal resistance.

WARNING

The Sample Processor does not provide sufficient protection during the

processing of potentially infectious samples or reagents.

Implement appropriate protective measures.

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