horiba Checker CC-100E Manuel utilisateur
Operating instructions
Converter Checker CC-100E
1.0 • 22.02.2021 •
HORIBA Table of contents
NOx Converter Checker CC-100E iii
Table of contents
1
General notes4
1.1
Address of the manufacturer4
1.2
Warranty and liability4
1.3
Trademark4
1.4
Applied EU directives and standards5
1.5
Intended use5
2
Security6
2.1
Spellings used6
2.2
General safety instructions6
3
Device overview9
3.1
Scope of delivery9
3.2
Labelling9
3.3
Description9
3.4
Unit views10
4
Installation and commissioning12
4.1
Before installation12
4.2
Environmental conditions13
4.3
Installation13
5
Operation14
5.1
Operation15
5.2
Relationship between ozone generation andNOxconcentration18
6
Maintenance19
6.1
Safety instructions for maintenance19
6.2
Maintenance plan19
6.3
Troubleshooting19
6.4
Spare parts20
7
Decommissioning21
8
Disposal22
9
Appendix22
9.1
Technical data22
9.2
Flow chart24
General notes
HORIBA
4/ 24 NOx Converter Checker CC-
100E
1 General information
Copyright© 2021 HORIBA Europe GmbH, all rights reserved.
This manual describes the operation of the NOx Converter Checker CC-100E (with integrated ozone
generator), which can be used to check the efficiency of NOx-to-NO converters used in gas analysers
during emission measurements or for process gas analysis.
Be sure to read this manual before using the product to ensure proper and safe operation of the unit.
Keep the manual in a safe place so that it is always available when needed.
Product specifications and the appearance and contents of this manual are subject to change without
notice.
All procedures and illustrations described in this manual refer to a unit with specific features. Please note
that your unit may differ. If you have any questions, please contact us.
1.1 Address of the manufacturer
HORIBA Europe GmbHHans-Mess-Straße
661440 Oberursel / Germany
Phone: +49 6172 1396 0Fax:
+49 6172 137 385E-mail
:
info.he@horiba.comInternet: www.horiba.com
1.2 Warranty and liability
The appliance is supplied by HORIBA with a warranty for a period of one (1) year.
In case of malfunction or damage within this year attributable to HORIBA, please contact HORIBA.
The warranty does not cover the following situations:
– Any malfunction resulting from improper operation.
– Any malfunction due to modifications or repairs not having been carried out or authorised by HORIBA.
– Any malfunction due to the use of the unit in an unsuitable environment.
– Any malfunction resulting from failure to observe the instructions in this operating manual.
– Any malfunction resulting from use of the appliance that does not comply with the instructions in this
manual.
– Any disruption resulting from natural disasters, accidents or breakdowns in which HORIBA is not
involved.
– Any malfunction due to the unit falling down.
– Signs of use such as rust etc. that are due to corrosion.
– consumables and the replacement of wear parts.
HORIBA is not liable for any damage caused by any malfunction of this product, any deletion of data, or any
other use of this product.
1.3 Trademarks
In general, company and brand names are either registered trademarks or trademarks of the respective
companies.
HORIBA General notes
NOx Converter Checker CC-100E 5/ 24
1.4 Applied EU directives and standards
This appliance complies with the following directives and standards:
Directive 2014/35/EU of the European Parliament and of the Council of 26 February 2014 on the
harmonisation of the laws of Member States relating to the making available
on the market of electrical equipment designed for use within certain voltage
limits (Low Voltage Directive)
Directive 2014/30/EU of the European Parliament and of the Council of 26 February 2014 on the
harmonisation of the laws of the Member States relating to electromagnetic
compatibility (EMC Directive)
EN 61010-1:2011-07 Safety requirements for electrical equipment for measurement, control, and
laboratory use - Part 1: General requirements
EN 61326-1:2013-07 Electrical equipment for measurement, control and laboratory use - EMC
requirements - Part 1: General requirements - Part 1: General requirements
1.5 Intended use
HORIBA's CC-100E is used to check the efficiency of the conversion of NOx to NO, as is common in NOx
analysers in flue gas analysis or process gas measurement. By means of ozone production through high-
voltage discharge and mixing with externally supplied nitrogen monoxide (NO), exact NO2 concentrations
are generated in a short reaction time.
Security HORIBA
6/ 24 NOx Converter Checker CC-100E
2 Safety
2.1 Spellings used
Warnings used in these operating instructions consist of a signal word, a warning, mandatory or instruction
symbol, the type of hazard incl. consequences and the instructions for avoiding it.
indicates an imminently hazardous situation which, if not avoided, will result in death
or serious injury.
Indicates a potentially hazardous situation which, if not avoided, could result in death
or serious injury.
indicates a potentially hazardous situation which, if not avoided, may result in minor or
moderate injury or property damage.
indicates
important information about the product or actions that must be observed for
the correct functioning of the unit.
The following symbols are used in these operating instructions and to identify hazardous points on the
system:
Symbol
Meaning
Warning of a general danger
Warning of electrical voltage
Hot surface warning
General note
2.2 General safety instructions
Target group
These instructions are intended for skilled personnel who are familiar with the general hazards involved in
the installation, maintenance and operation of equipment in commercial or industrial environments.
Before installation and first commissioning, the personnel must obtain knowledge of the intended use of
the system by carefully reading these operating instructions.
– Operation - instructed competent personnel with required expertise
– Maintenance - qualified personnel with required knowledge, electrician
The warnings must be observed.
HORIBA
Security
NOx Converter Checker CC-100E 7/ 24
Electrical safety
DANGER
Electrical voltage
Danger of electric shock
There are parts in the unit that are under dangerous voltage
a) The unit may only be opened by instructed, skilled personnel.
b) Disconnect the unit from the mains at all poles when carrying out maintenance
work on electrical components. To do this, pull out the mains plug. Simply
switching off the unit at the mains switch is not sufficient!
c) Secure the unit against unintentional restart.
d)
Work on the opened device when it is live may only be carried out by a specialist
who is familiar with the associated dangers.
Switch off in an emergency
WARNING
Emergency
Uncontrollable operation of the appliance, occurrence of fire and smoke.
a) Switch off the unit and disconnect the mains plug.
b)
Close the valves on the gas cylinders or the external feeds.
Hazardous substances
WARNING
Toxic gases
The unit handles toxic gases. Uncontrolled leakage of these gases can cause a
serious accident such as poisoning.
a) Connect the system according to this manual.
b) Use the specified connections as well as hoses and pipes and connect them
gas-tight.
c) Check that the applied gas pressure corresponds to the nominal value.
d)
Ensure that your working environment is properly ventilated.
CAUTION
Handling auxiliary materials and consumables
Auxiliary materials and consumables may contain substances that are
hazardous to health or the environment.
a) Follow the instructions for action written in the safety data sheets of the
auxiliary materials and consumables.
b)
Wear your personal protective equipment if necessary.
Security HORIBA
8/ 24 NOx Converter Checker CC-100E
The following safety instructions are on the unit:
Reverse side:
HORIBA Device overview
NOx Converter Checker CC-100E 9/ 24
3 Unit overview
3.1 Scope of delivery
Designation
Quantity
NOx Converter Checker CC-100E
1 piece
Operating instructions
1 piece
Mains connection cable 230V
1 piece
3.2 Labelling
Fig. 1:
Example of a type plate
The nameplate of the CC-100E is located on the back above the O2 inlet.
3.3 Description
The HORIBA Converter Checker CC-100E is a compact device for checking the reliability of gas analysers
for determining the NOx content in exhaust gases. For this purpose, the device generates ozone from an
oxygen-saturated atmosphere in a high-voltage unit, mixes the ozone with externally supplied NO and
produces a gas mixture with a precise NO2 concentration. The CC-100E is optimised for high stability and
short reaction times.
The operating principle of the NOx Converter-Checker CC-100E is based on gas phase titration (GPT). Gas
phase titration generally refers to any titration carried out in the gas phase. More specifically, it is a method
for determining reactive fractions in the gas phase by reacting with the excess of another gas that serves
as the titrant. In our case, the gaseous analyte is ozone, which can be "titrated" with nitric oxide according
to the following reaction
O3 + NO → O2 + NO2.
The unknown NO concentration can then be determined from measuring the concentration of the reaction
products.
Compared to simple spectrophotometry, gas phase titration has two advantages:
The measurement is not dependent on the path length of the gas path, as the same gas path is used for
both the measurement of the excess titrant and the measurement of the product.
The measurement also does not depend on the linear change in absorbance as a function of the
concentration of the gas to be analysed (Beer-Lambert law). Therefore, the method is particularly suitable
for such samples whose components interfere at similar wavelengths as the analysis gas.
Device overview HORIBA
10/ 24 NOx Converter Checker CC-100E
3.4 Unit views
Front view
Fig. 2:
Front view
Position
Designation
1
ON/OFF switch
2
Touch screen for operation
3
USB 1 (not in use)
4
USB 2 (service interface for updating the firmware)
Rear view
Fig. 3:
Rear view
Position
Designation
1
Oxygen inlet for ozone generation (inlet valve 1)
2
Nitrogen inlet as reference (inlet valve 2)
3
NO Calibration gas inlet (inlet valve 3)
4
Connection to the gas inlet of the analyser
5
Mains connection (Power)
6
RS232 interface
7
Bypass
HORIBA Device overview
NOx Converter Checker CC-100E 11/ 24
Interior view
Fig. 4:
Interior view
Position
Designation
1
Inlet valve 1; oxygen inlet
2
Inlet valve 2; nitrogen inlet
3
Inlet valve 3; Calibration gas (NO) inlet
4
Output to the analyser
5
Mains connection
6
RS232 interface
7
Bypass
8
Power supply unit
9
Mixing area
10
Pressure regulator 2
11
Capillary line 2
12
Pressure regulator 1
13
Capillary line 1
14
Ozone generator
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