Hach TitraLab AT1102 Manuel utilisateur

DOC022.52.93074
TitraLab® AT1000 series workstations
User Manual
03/2019, Edition 7


Table of Contents
Section 1 Specifications.................................................................................................................... 3
Section 2 General information......................................................................................................... 5
2.1 Safety information........................................................................................................................ 5
2.1.1 Use of hazard information................................................................................................... 5
2.1.2 Precautionary labels............................................................................................................ 5
2.1.3 Certification......................................................................................................................... 6
2.1.4 Restriction of hazardous substances (RoHS)..................................................................... 6
2.2 Product overview.......................................................................................................................... 7
2.3 Instrument connections................................................................................................................ 9
2.4 Product components.................................................................................................................... 9
Section 3 Installation........................................................................................................................ 11
3.1 Installation guidelines................................................................................................................. 11
3.2 Connect to AC power................................................................................................................. 11
3.3 Install the syringe....................................................................................................................... 12
3.4 Install the sensor storage tubes................................................................................................. 13
3.5 Install the stir bar and the beaker............................................................................................... 13
3.6 Prepare the tubes....................................................................................................................... 13
3.7 Connect the tubes...................................................................................................................... 14
3.8 Install the sensor........................................................................................................................ 14
3.8.1 Install the legacy adapter.................................................................................................. 14
3.8.1.1 Set the legacy adapter settings................................................................................ 15
3.8.2 Connect the sensor........................................................................................................... 15
3.9 Install the titrant and the reagent................................................................................................ 16
3.10 Tidy the work area.................................................................................................................... 17
Section 4 Install accessories..........................................................................................................19
4.1 Install an external pump............................................................................................................. 19
4.2 Install an external propeller........................................................................................................ 21
4.3 Install a balance......................................................................................................................... 21
4.4 Install PC software..................................................................................................................... 22
4.5 Install the syringe verification kit................................................................................................ 22
Section 5 User interface and navigation......................................................................................25
5.1 Keypad....................................................................................................................................... 25
5.2 Home screen.............................................................................................................................. 25
5.3 Menu structure........................................................................................................................... 26
Section 6 Startup............................................................................................................................... 29
6.1 Configure the instrument............................................................................................................ 29
6.2 Install the applications................................................................................................................ 30
6.3 Prepare the instrument for measurement.................................................................................. 30
Section 7 Standard operations...................................................................................................... 33
7.1 Calibration.................................................................................................................................. 33
7.1.1 Calibrate the sensor.......................................................................................................... 33
7.1.2 Calibrate the titrant............................................................................................................ 34
7.1.3 Auto leveling calibration.................................................................................................... 35
7.2 Sample preparation.................................................................................................................... 36
7.3 Get a sample measurement....................................................................................................... 36
7.4 Change the application settings................................................................................................. 38
7.4.1 Sample name.................................................................................................................... 38
7.5 Manage the data log.................................................................................................................. 39
7.6 Purge..........................................................................................................................................39
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Section 8 Maintenance..................................................................................................................... 41
8.1 Maintenance schedule............................................................................................................... 41
8.2 Clean the instrument.................................................................................................................. 41
8.3 Clean the sensor........................................................................................................................ 41
8.4 Replace the tubes...................................................................................................................... 42
8.5 Replace desiccant cartridge contents........................................................................................ 42
8.6 Replace the syringe electro-valve block..................................................................................... 42
8.7 Maintenance menu..................................................................................................................... 42
8.7.1 Syringe activation.............................................................................................................. 43
8.7.2 Pump activation................................................................................................................. 43
8.7.3 Syringe management........................................................................................................ 43
8.7.4 Syringe verification............................................................................................................ 43
8.7.5 Pump cassette replacement.............................................................................................. 44
8.7.6 Other maintenance options............................................................................................... 45
8.8 Storage and transportation......................................................................................................... 46
8.8.1 Prepare the instrument for storage....................................................................................46
8.8.2 Prepare the instrument for short-term storage.................................................................. 47
8.8.3 Prepare the instrument for shipment................................................................................. 47
Section 9 Troubleshooting..............................................................................................................49
Section 10 Replacement parts and accessories........................................................................57
Appendix A Change application parameters.............................................................................. 63
Appendix B Frequently asked questions.................................................................................... 73
Section 13 Configure the instrument........................................................................................... 75
Table of Contents
2

Section 1 Specifications
Specifications are subject to change without notice.
Specification Details
Dimensions (W x D x H) 22 x 40 x 36 cm (8.7 x 15.7 x 14.2 in.)
Weight 4 kg (8.8 lb)
Power requirements 100–240 VAC, 50/60 Hz
Altitude 2,000 m (6,562 ft) maximum
Operating temperature 15 to 35 °C (59 to 95 °F)
Relative humidity 20 to 80%, non-condensing
Storage temperature –5 to 40 °C (23 to 104 °F)
Installation category II
Pollution degree 2
Certifications Safety IEC/EN 61010-1; EMC IEC/EN 61326-1
EMC requirements This product is intended to be used in a domestic or basic
electromagnetic environment
Warranty 1 year (EU: 2 years)
3

Specifications
4

Section 2 General information
In no event will the manufacturer be liable for direct, indirect, special, incidental or
consequential damages resulting from any defect or omission in this manual. The
manufacturer reserves the right to make changes in this manual and the products it
describes at any time, without notice or obligation. Revised editions are found on the
manufacturer’s website.
2.1 Safety information
NOTICE
The manufacturer is not responsible for any damages due to misapplication or misuse of this
product including, without limitation, direct, incidental and consequential damages, and disclaims
such damages to the full extent permitted under applicable law. The user is solely responsible to
identify critical application risks and install appropriate mechanisms to protect processes during a
possible equipment malfunction.
Please read this entire manual before unpacking, setting up or operating this equipment.
Pay attention to all danger and caution statements. Failure to do so could result in serious
injury to the operator or damage to the equipment.
Make sure that the protection provided by this equipment is not impaired. Do not use or
install this equipment in any manner other than that specified in this manual.
2.1.1 Use of hazard information
DANGER
Indicates a potentially or imminently hazardous situation which, if not avoided, will result in death
or serious injury.
WARNING
Indicates a potentially or imminently hazardous situation which, if not avoided, could result in
death or serious injury.
CAUTION
Indicates a potentially hazardous situation that may result in minor or moderate injury.
NOTICE
Indicates a situation which, if not avoided, may cause damage to the instrument. Information that
requires special emphasis.
2.1.2 Precautionary labels
Read all labels and tags attached to the instrument. Personal injury or damage to the
instrument could occur if not observed. A symbol on the instrument is referenced in the
manual with a precautionary statement.
This symbol, if noted on the instrument, references the instruction manual for operation and/or safety information.
This symbol indicates that a risk of electrical shock and/or electrocution exists.
5

This symbol indicates the presence of devices sensitive to Electro-static Discharge (ESD) and indicates that care
must be taken to prevent damage with the equipment.
Electrical equipment marked with this symbol may not be disposed of in European domestic or public disposal
systems. Return old or end-of-life equipment to the manufacturer for disposal at no charge to the user.
2.1.3 Certification
CAUTION
This equipment is not intended for use in residential environments and may not provide adequate
protection to radio reception in such environments.
Canadian Radio Interference-Causing Equipment Regulation, IECS-003, Class A:
Supporting test records reside with the manufacturer.
This Class A digital apparatus meets all requirements of the Canadian Interference-
Causing Equipment Regulations.
Cet appareil numérique de classe A répond à toutes les exigences de la réglementation
canadienne sur les équipements provoquant des interférences.
FCC Part 15, Class "A" Limits
Supporting test records reside with the manufacturer. The device complies with Part 15 of
the FCC Rules. Operation is subject to the following conditions:
1. The equipment may not cause harmful interference.
2. The equipment must accept any interference received, including interference that
may cause undesired operation.
Changes or modifications to this equipment not expressly approved by the party
responsible for compliance could void the user's authority to operate the equipment. This
equipment has been tested and found to comply with the limits for a Class A digital
device, pursuant to Part 15 of the FCC rules. These limits are designed to provide
reasonable protection against harmful interference when the equipment is operated in a
commercial environment. This equipment generates, uses and can radiate radio
frequency energy and, if not installed and used in accordance with the instruction manual,
may cause harmful interference to radio communications. Operation of this equipment in
a residential area is likely to cause harmful interference, in which case the user will be
required to correct the interference at their expense. The following techniques can be
used to reduce interference problems:
1. Disconnect the equipment from its power source to verify that it is or is not the source
of the interference.
2. If the equipment is connected to the same outlet as the device experiencing
interference, connect the equipment to a different outlet.
3. Move the equipment away from the device receiving the interference.
4. Reposition the receiving antenna for the device receiving the interference.
5. Try combinations of the above.
2.1.4 Restriction of hazardous substances (RoHS)
Dieses Informationsblatt enthält Angaben, die ausschließlich für den Export dieses
Gerätes in die Volksrepublik China erforderlich sind.
This document contains information which is only required for the export of this
instrument into the People's Republic of China.
本手册包含的必要信息只适用于出口到中华人民共和国的仪器。
Type: AT1xxx
General information
6

Name: TitraLab AT1000
Table 1 有毒有害物质或元素 (Hazardous Substance)
部件名称 (Parts) 铅 (Pb) 汞 (Hg) 镉 (Cd) 六价铬 (Cr6+) 多溴联苯 (PBB) 多溴二苯醚 (PBDE)
电 阻 (Resistor) X O O O O O
二极管 ( Diode) X O O O O O
O:
表示该部件中有毒有害物质在所有均质材料中的含量均为 SJ/T11363-2006 标准规定的限量要求以下
Indicates that the concentration of the hazardous substance in all homogeneous materials in the parts is below the
relevant threshold of the SJ/T11363-2006 standard.
X:
表示该部件中有毒有害物质至少在某一均质材料中的含量超出 SJ/T11363-2006 标准规定的限量要求
Indicates that the concentration of the hazardous substance of at least one of all homogeneous materials in the parts
is above the threshold of the SJ/T11363-2006 standard.
对销售之日的所售产品, 本表显示, 朗讯供应链的电子信息产品可能包含这些物质。注意: 在所售产品中可能会也可能不会含有
所有所列的部件
This table shows where these substances may be found in the supply chain of "Company" electronic information products, as
of the date of sale of the enclosed product. Note that some of the component types listed above may or may not be a part of
the enclosed product.
除非另外特别的标注, 此标志为针对所涉及产品的环保使用期标志. 某些可更换的零部件会有一个不同的环保使用
期( 例如, 电池单元模块) 贴在其产品上. 此环保使用期限只适用于产品的手册中所规定的条件下工作.
The Environmentally Friendly Use Period (EFUP) for all enclosed products and their parts are per the symbol
shown here, unless otherwise marked. Certain field-replaceable parts have a different EFUP (for example,
battery modules) and so are marked to reflect such. The Environmentally Friendly Use Period is valid only
when the product is operated under the conditions defined in the product manual.
2.2 Product overview
The instrument operates with digital and analog sensors. Measurement applications are
installed on the instrument to automate the measurement process. Instructions show on
the display when user intervention is required.
General information
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1 Keypad 6 Beaker 11 Sensor holder
2 Display 7 Syringe protection cover 12 Pump 2 input/output
3 Sensor storage tubes 8 Syringe input/output 13 Pump 1 input/output
4 USB port19 Tube clips 14 Pump access cover
5 Tube holder 10 Syringe
Note: Depending on the model, there will be 1 or 2 syringes and syringe input/output ports, and 0,
1 or 2 pumps. Refer to Table 2.
Table 2 Instrument configurations
Model Syringes Pumps
AT1102 1 0
AT1112 1 1
AT1122 1 2
AT1222 2 2
1A second USB port is found on the rear of the instrument, but the instrument recognizes only one USB storage
device connection at a time.
General information
8
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