Fritsch PULVERISETTE 7 premium line Manuel utilisateur

Operang instrucons

PLANETARY MICRO MILL

PULVERISETTE 7

premium line

Read the instrucons prior to performing any task!

Valid starng with: 07.5000/00100

Translaon of the original operang instrucons

Version 05/2022 Index 032

Fritsch GmbH

Milling and Sizing

Industriestraße 8

D - 55743 Idar-Oberstein

Telephone: +49 6784 70-0

Email: inf[email protected]

Internet: www.fritsch.de

Cercaons and CE conformity

Cercaon

CE Conformity

Cercaons and CE conformity

Fritsch GmbH has been cered by the SGS-TÜV Saar GmbH.

An audit cered that Fritsch GmbH conforms to the requirements of the DIN EN

ISO 9001:2015.

The enclosed Conformity Declaraon lists the guidelines the FRITSCH instrument

conforms to, to be able to bear the CE mark.

Table of contents

1 Safety informaon and use. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8

1.1 Requirements for the user. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8

1.2 Scope of applicaon. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8

1.2.1 Operang principle. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9

1.2.2 Drive motor and speed regulaon. . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9

1.3 Obligaons of the operator. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9

1.4 Informaon on hazards and symbols used in this manual. . . . . . . . . . . . 10

1.5 Informaon on hazards at the device. . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12

1.6 Device safety informaon. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12

1.7 Protecve equipment. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14

1.8 Hazardous points. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15

1.9 Electrical safety. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15

1.9.1 General informaon. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15

1.9.2 Protecon against restart. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15

1.9.3 Overload protecon. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16

1.9.4 Imbalance detecon. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16

2Technical data. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17

2.1 Dimensions. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17

2.2 Weight. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17

2.3 Operang noise. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17

2.4 Voltage. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17

2.5 Current consumpon. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17

2.6 Protecon class. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17

2.7 Power consumpon. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17

2.8 Electrical fuses. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17

2.9 Material. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 18

2.10 Final neness. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 18

3Installaon. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19

3.1 Transport. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19

3.2 Unpacking. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19

3.3 Seng up. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20

3.4 Ambient condions. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20

3.5 Electrical connecon. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21

Table of contents

4Inial start-up. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 22

4.1 Switching on. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 22

4.2 Funcon check. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 22

4.3 Switching o. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 24

5 Using the device. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 25

5.1 Safety informaon. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 25

5.1.1 General informaon. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 26

5.1.2 Overpressure relief of the grinding bowls. . . . . . . . . . . . . . . . . . . . . . . 26

5.1.3 Grinding bowl lid. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 28

5.2 Choice of grinding bowls and grinding balls. . . . . . . . . . . . . . . . . . . . . . . . 29

5.2.1 Size of the grinding balls. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 30

5.2.2 Number of balls per grinding bowl (independent of the material

quanty). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 31

5.2.3 Calculated weight of a ball. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 32

5.3 Impact of the ball size and the material during grinding. . . . . . . . . . . . . 32

5.4 Filling quanes of grinding bowls. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 33

5.5 Filling the grinding bowl. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 34

5.6 Factors with an impact on grinding. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 34

5.6.1 Running me (grinding duraon). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 34

5.6.2 Speed. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 34

5.6.3 Reverse mode. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35

5.6.4 Number and size of the balls. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35

5.6.5 Weight of the balls (type of material). . . . . . . . . . . . . . . . . . . . . . . . . . 35

5.7 Dry grinding. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35

5.8 Wet grinding (grinding in a suspension). . . . . . . . . . . . . . . . . . . . . . . . . . . 36

5.8.1 The eect of high temperature. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 37

5.8.2 Safety measures against an excessively high pressure. . . . . . . . . . . . . 37

5.9 Handling the grinding bowl. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 38

5.9.1 Design. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 38

5.9.2 Opening the grinding bowl aer a grinding operaon. . . . . . . . . . . . . 38

5.9.3 Closing the grinding bowl. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 40

5.9.4 Inserng the grinding bowl in the grinding bowl holder. . . . . . . . . . . 42

5.9.5 Removing the grinding bowl. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 43

5.10 Mass balance. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 45

5.11 Grinding duraon. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 45

5.12 Conducng a grinding operaon. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 46

5.12.1 Program sequence aer switching on. . . . . . . . . . . . . . . . . . . . . . . . . . 46

5.12.2 Starng grinding at high speed. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 49

Table of contents

5.12.3 Overload. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 50

5.12.4 "Program" menu item. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 50

5.12.5 Saving the current data. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 51

5.12.6 Loading the program. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 52

5.12.7 Seng the me control. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 52

5.12.8 Imbalance check. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 54

5.12.9 Switching o. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 55

5.12.10 Cooling the grinding bowl. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 55

6Accessories. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 56

6.1 Standard gassing lid for grinding with inert gas. . . . . . . . . . . . . . . . . . . . . 56

6.1.1 Scope of delivery. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 56

6.1.2 Fing the gassing lid on the grinding bowl. . . . . . . . . . . . . . . . . . . . . . 57

6.1.3 Hose adapter for grinding bowl gassing. . . . . . . . . . . . . . . . . . . . . . . . . 59

6.1.4 Removing the gassing lid in individual steps. . . . . . . . . . . . . . . . . . . . . 60

6.2 Gassing lid with stainless steel, swagelok hose couplings. . . . . . . . . . . . . 62

6.2.1 Scope of delivery / lid design. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 63

6.2.2 Fing the gassing lid on the grinding bowl. . . . . . . . . . . . . . . . . . . . . . 63

6.2.3 Hose adapter for grinding bowl gassing. . . . . . . . . . . . . . . . . . . . . . . . . 65

6.2.4 Removing the gassing lid in individual steps. . . . . . . . . . . . . . . . . . . . . 66

6.3 EASY GTM Gas Pressure and Temperature Measuring System. . . . . . . . . 67

6.3.1 Case contents and system design. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 67

6.3.2 Inserng / changing the baery. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 67

6.3.3 Conguraon of transmier ID and data transmission frequency. . . 70

6.3.4 Installaon of the transmission unit on the EASY GTM bowl. . . . . . . . 71

6.3.5 Installaon of the receiver board in the P-7 premium line. . . . . . . . . . 73

6.3.6 Acvang EASY GTM. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 74

6.3.7 Entering the temperature limit. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 75

6.3.8 Entering the pressure limit. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 76

6.3.9 Selecng the operang mode. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 77

6.3.10 Deacvang EASY GTM. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 77

6.3.11 Cleaning the EASY GTM system. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 78

6.3.12 Baery arrangement. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 80

6.4 Special emptying device for grinding bowls. . . . . . . . . . . . . . . . . . . . . . . . 80

6.4.1 Design. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 81

6.4.2 Handling. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 81

6.4.3 Cleaning the special emptying device. . . . . . . . . . . . . . . . . . . . . . . . . . 84

Table of contents

6.5 Compl. counterweight. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 84

6.5.1 Design. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 84

6.5.2 Handling. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 85

6.6 Planetary mills - "MillControl" soware. . . . . . . . . . . . . . . . . . . . . . . . . . . 86

6.7 Single-use grinding containers. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 86

7 General and oponal sengs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 88

7.1 Standard Operaon Procedure. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 88

7.1.1 Acvang SOP mode. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 89

7.1.2 Deacvang SOP mode. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 89

7.1.3 Deleng SOP mode. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 90

7.2 RFID. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 90

7.3 Language change. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 91

7.4 Screen brightness. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 92

7.5 Informaon. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 93

7.6 Interfaces. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 94

7.7 Firmware update. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 95

8 Cleaning. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 96

8.1 Grinding elements. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 96

8.2 Mill. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 96

8.2.1 Removing the grinding chamber cover. . . . . . . . . . . . . . . . . . . . . . . . . 97

9 Maintenance. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 98

10 Guarantee terms. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 99

11 Exclusion of liability. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 101

12 Safety logbook. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 103

13 Index. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 105

Safety informaon and use

1 Safety informaon and use

1.1 Requirements for the user

This operang manual is intended for persons assigned with operang and mon-

itoring the Fritsch PULVERISETTE 7 premium line. The operang manual and

especially its safety instrucons are to be observed by all persons working on

or with this device. In addion, the applicable rules and regulaons for accident

prevenon at the installaon site are to be observed. Always keep the operang

manual at the installaon site of the PULVERISETTE 7 premium line.

People with health problems or under the inuence of medicaon, drugs, alcohol

or exhauson must not operate this device.

The PULVERISETTE 7 premium line may only be operated by authorised persons

and serviced or repaired by trained specialists. All commissioning, maintenance

and repair work may only be carried out by technically qualied personnel.

Qualied personnel are persons who, because of their educaon, experience and

training as well as their knowledge of relevant standards, regulaons, accident

prevenon guidelines and operang condions, are authorised by those respon-

sible for the safety of the machine to carry out the required work and are able to

recognize and avoid possible hazards as dened for skilled workers in IEC 364.

In order to prevent hazards to users, follow the instrucons in this manual.

Malfuncons that impair the safety of persons, the PULVERISETTE 7 premium

line or other material property must be reced immediately. The following

informaon serves both the personal safety of operang personnel as well as

the safety of the products described and any devices connected to them: All

maintenance and repair work may only be performed by technically qualied

personnel.

This operang manual is not a complete technical descripon. Only the details

required for operaon and maintaining usability are described.

Fritsch has prepared and reviewed this operang manual with the greatest care.

However, no guarantee is made for its completeness or accuracy.

Subject to technical modicaons.

1.2 Scope of applicaon

NOTICE

This laboratory instrument is designed for an 8-hour shi oper-

aon at 30 % duty cycle and not for connuous operaon.

The duty cycle is dened as the rao of load duraon to run

me. The run me is dened as load duraon plus pause me.

According to DIN EN 60034-1 (VDE 0530, IEC34-1) a connuous

operaon already takes place aer a standardised run me of

10 minutes. At 30 % duty cycle (DC = rao of load duraon to

run me) a load duraon of 3 minutes and a pause me of 7

minutes would be within standard.

If the standardised run me of 10 minutes is exceeded, then,

by denion, there would be a connuous operaon and

disproporonate temperature increases may occur, possibly

involving increased wear.

Safety informaon and use

The planetary micro mill, "PULVERISETTE 7 premium line", can be applied univer-

sally for the fast dry or wet grinding of inorganic and organic samples for analysis,

quality inspecon or material tesng.

During synthesis, the planetary micro mill is used for mixing and homogenizaon

of dry samples, emulsions or suspensions.

The planetary micro mill,

premium line

, described here is an equipment item for

use in industrial environments.

The device may be used for these purposes only.

1.2.1 Operang principle

aRotaon of the grinding bowl

b Centrifugal force

cRotaon of the support disc

The source material is crushed and ground by grinding balls in a grinding bowl.

The centrifugal forces from the rotaon of the grinding bowls around their own

axis and from the rotang support disc have an eect on the contents of the

grinding bowl, consisng of material to be ground and grinding balls.

The grinding bowl and the support disc have opposite direcons of rotaon,

in order that the centrifugal forces alternate in the same direcon and in the

opposite direcon.

The result is that the grinding balls run down the inside of the bowl's wall with

a fricon eect and the grinding balls hit the opposite wall of the grinding bowl

with an impact eect.

1.2.2 Drive motor and speed regulaon

A maintenance-free electric motor operated via frequency converter is used as

the drive.

1.3 Obligaons of the operator

Before using the PULVERISETTE 7 premium line, this manual is to be carefully

read and understood. The use of the PULVERISETTE 7 premium line requires

technical knowledge; only commercial use is permied.

The operang personnel must be familiar with the content of the operang

manual. For this reason, it is very important that these persons actually receive

the present operang manual. Ensure that the operang manual is always near

the device.

The PULVERISETTE 7 premium line may exclusively be used within the scope of

applicaons set down in this manual and within the framework of guidelines put

forth in this manual. In case of non-compliance or improper use, the customer

assumes full liability for the funconal capability of the PULVERISETTE 7 premium

line and for any damage or injury arising from failure to full this obligaon.

By using the PULVERISETTE 7 premium line the customer agrees with this and

recognizes that defects, malfuncons or errors cannot be completely excluded.

To prevent risk of damage to persons or property or of other direct or indirect

damage, resulng from this or other causes, the customer must implement su‐

cient and comprehensive safety measures for working with the PULVERISETTE 7

premium line.

Safety informaon and use

Special safety informaon

Neither compliance with this manual nor the condions and methods used

during installaon, operaon, use and maintenance of the PULVERISETTE 7

premium line can be monitored by Fritsch GmbH. Improper execuon of the

installaon can result in property damage and thus endanger persons. Therefore,

we assume absolutely no responsibility or liability for loss, damage or costs

that result from errors at installaon, improper operaon or improper use or

improper maintenance or are in any way connected to these.

The applicable accident prevenon guidelines must be complied with.

Generally applicable legal and other obligatory regulaons regarding environ-

mental protecon must be observed.

1.4 Informaon on hazards and symbols used in this manual

Safety informaon

Safety informaon in this manual is designated by symbols. Safety informaon is

introduced by keywords that express the extent of the hazard.

DANGER

This symbol and keyword combinaon points out a directly

hazardous situaon that can result in death or serious injury if

not avoided.

WARNING

This symbol and keyword combinaon points out a possibly

hazardous situaon that can result in death or serious injury if

not avoided.

CAUTION

This symbol and keyword combinaon points out a possibly

hazardous situaon that can result in slight or minor injury if

not avoided.

NOTICE

This symbol and keyword combinaon points out a possibly

hazardous situaon that can result in property damage if not

avoided.

To call aenon to specic hazards, the following symbols are used in the safety

informaon:

DANGER

This symbol and keyword combinaon points out a directly haz-

ardous situaon due to electrical current. Ignoring informaon

with this designaon will result in serious or fatal injury.

Autres manuels pour PULVERISETTE 7 premium line

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