Distek Evolution 6300 Manuel utilisateur

Operation

Manual

Evolution

Dissolution Test

System

6100

6300

Evolution Dissolution Test System

Operation Manual

Document # 3861-0001



Distek, Inc.

121 Nort Center Dr. • Nort Brunswick, NJ 08902

P one 732.422.7585 • Fax 732.422.7310

ttp://www.distekinc.com

Notice

This document contains proprietary information. All ri hts are

reserved. No part of this document may be photocopied,

reproduced or translated without the prior written consent of

Distek, Inc.

121 North Center Drive

North Brunswick, NJ 08902-4905

Tel. (732) 422-7585

Fax. (732) 422-7310

Website: http://www.distekinc.com

“Dow Corning” is a registered trademark of Dow Corning Corporation, USA.

CenterC ek, Heig tC ek, RPMC ek, S aftC ek and TempC ek are trademarks of Distek,

Inc.

T e Distek logo is a registered trademark of Distek, Inc.

All ot er company and product names are trademarks or registered trademarks of t eir

respective olders.

Document Revision History

Rev Date Notes

A June 2003 Initial Release

B December 2003 See Distek C ange Notice 0405

C October 2004 Updated for Firmware Rev. 2.13. See Distek C ange Notice

0456.

D June 2005 Updated Appendix A: Spare Parts & Accessories. See Distek

C ange Notice 0508.

E September 2005

Removed Certificate of Compliance from Manual. Certificate

is a separate file on manual CD. See C ange Notice 0516.

Page B-1: Step # 5.3 – c ange “0.3V” to “2.0 V” and “0.5 V”

to “3.0 V”

Page D-2 and D-3 – add note to bottom of page - “Asterisk (*)

in Temperature Profiles denotes out of USP specification”

F May 2007 See Distek C ange Notice 0580. Updated for FW Rev. 2.15.

Operation Manual: Evolution Series

Contents

About this Manual......................................................................... i

Purpose .................................................................................. ii

Audience ................................................................................ ii

Contents................................................................................. ii

Prerequisites............................................................................iii

Documentation .........................................................................iii

Conventions.............................................................................iii

1Introduction ..................................................................... 1-1

Overview .............................................................................. 1-2

Specification.......................................................................... 1-2

P ysical Site Considerations........................................................ 1-4

Environmental Considerations ..................................................... 1-5

Distek & t e WEEE Directive (Waste Electrical & Electronic Equipment) 1-5

Ambient Laboratory Temperatures ............................................. 1-5

Ambient Laboratory Humidity ................................................... 1-6

Air Quality Considerations ....................................................... 1-7

Operation Warnings and Notes..................................................... 1-8

General Instrument Overview .....................................................1-11

2Installation....................................................................... 2-1

Unpacking ............................................................................. 2-2

Leveling t e Evolution System ..................................................... 2-3

Installing t e T ermocirculator (Evolution 6300 Only) ......................... 2-6

Placement and Connections ..................................................... 2-7

Filling t e Water Bat ............................................................ 2-8

Priming t e Pump ................................................................. 2-8

Operation Manual: Evolution Series

Positioning t e Vessels .............................................................2-10

Paddle and Basket Installation ....................................................2-11

Paddle Blade Installation........................................................2-11

Basket Installation ...............................................................2-11

C ecking Paddles, Baskets and S afts for Straig tness.....................2-12

C ecking S aft Centering .......................................................2-12

Paddles and Basket Heig t Adjustment..........................................2-12

Initial Heig t Setting for Paddles and Baskets: ..............................2-13

Quick C ange Heig t Adjustment Knob (Paddles or Baskets)..............2-14

Installing t e Calibration Probe...................................................2-14

Installation C eckout...............................................................2-15

RPM Control .......................................................................2-15

Test Duration .....................................................................2-15

Temperature Control ............................................................2-16

Time and Date ....................................................................2-16

3Operation ........................................................................ 3-1

Control Keypad ....................................................................... 3-4

ESC/DEL Button.................................................................... 3-4

RUN/STOP Button ................................................................. 3-4

Arrow Keys ......................................................................... 3-4

ENTER Button ...................................................................... 3-4

+ Button ............................................................................ 3-5

- Button............................................................................. 3-5

Stir LED ............................................................................. 3-5

Heat LED............................................................................ 3-5

Sleep LED........................................................................... 3-5

produKEY ........................................................................... 3-5

Startup Screens....................................................................... 3-5

System Administration .............................................................. 3-6

System Setup....................................................................... 3-7

Advanced Options .............................................................. 3-8

Unit Address ..................................................................... 3-8

TCS Address (Evolution 6300 Only)........................................... 3-9

Pre eat (Evolution 6300 Only) ................................................ 3-9

Temperature Control (Evolution 6300 Only)............................... 3-10

Beep Mode ...................................................................... 3-10

Heig t Switc Setting ......................................................... 3-10

Printer S aring Configuration (Evolution 6100 Only) ..................... 3-11

About Window.................................................................. 3-12

User Configuration ...............................................................3-12

Creating a New Account ...................................................... 3-14

C anging t e Privileges of an Existing Account ........................... 3-15

C anging a Password .......................................................... 3-15

Deleting an Account........................................................... 3-16

Temperature Calibration........................................................3-16

Operation Manual: Evolution Series

Calibrate Using Evolution Calibration Probe............................... 3-18

Calibrate Using TempC ek Digital T ermometer ......................... 3-19

Calibrate Using NIST-Traceable Reference T ermometer ............... 3-19

Calibrate calPROBE Using TempC ek Digital T ermometer ............. 3-20

Calibrate calPROBE Using NIST-Traceable Reference T ermometer... 3-21

Display Screens ......................................................................3-21

Temperature Screen .............................................................3-21

Temperature and RPM Screen ..................................................3-22

Current Met od...................................................................3-23

Report History ....................................................................3-23

Printing a Saved Report .........................................................3-24

Working wit Met ods (Automatic Mode) .......................................3-24

Selecting a Met od to Run ......................................................3-24

Sorting t e Met od List..........................................................3-25

Programming a New Met od....................................................3-25

Running a Simultaneous Drop wit Paddles ..................................3-27

Running a Simultaneous Drop wit Baskets...................................3-28

Running a Staggered Drop wit Paddles ......................................3-28

Running a Staggered Drop wit Baskets.......................................3-28

Open/View an Existing Met od.................................................3-29

Modify a Saved Met od ..........................................................3-30

Deleting a Met od................................................................3-30

Copy a Saved Met od to a New Name.........................................3-30

Printing Met od Parameters....................................................3-31

Working in Manual Mode ...........................................................3-31

Controlling Vessels Individually (Evolution 6100 Only) .....................3-32

Controlling All Vessels ...........................................................3-33

TCS Activation (Evolution 6300 Only) .........................................3-35

Running a Manual Mode Test ...................................................3-35

Using t e produKEY.................................................................3-36

Saving a Met od to t e produKEY..............................................3-36

Viewing Met ods on t e produKEY.............................................3-37

Saving a Met od from t e produKEY to t e Instrument ....................3-37

Running a Met od from t e produKEY ........................................3-37

Deleting Met ods from t e produKEY .........................................3-38

Printing a Met od from t e produKEY.........................................3-38

Using a Premiere 5100 produKEY ..............................................3-38

Using t e calKEY ....................................................................3-38

Storing Calibration Data.........................................................3-39

Restoring Calibration Data ......................................................3-39

Printouts..............................................................................3-40

Serial Port Control ..................................................................3-40

4Maintenance..................................................................... 4-1

General Information ................................................................. 4-2

Emptying t e Water Bat & TCS (Evolution 6300 Only) ........................ 4-3

Removing t e Water Bat (Evolution 6300 Only)................................ 4-4

Operation Manual: Evolution Series

Re-installing t e Water Bat (Evolution 6300 Only) ............................ 4-5

Replacing t e Water Bat and TCS Tubing (Evolution 6300 Only) ............ 4-5

5Troubles ooting................................................................. 5-1

Troubles ooting ...................................................................... 5-2

Error Messages.......................................................................5-15

Warning Messages...................................................................5-17

General Messages ...................................................................5-18

Service................................................................................5-19

Appendix A : Spare Parts and Accessories ...................................... A-1

Appendix B : Pre-Installation Considerations: Electrical Power SupplyB-1

Appendix C : CE Declaration of Conformity .................................... C-1

Appendix D : Sample Printouts from Parallel Printer ......................... D-1

About T is Manual

Operation Manual: Evolution Series

About this Manual

About T is Manual includes information about w at is contained in t is manual and

t e conventions used.

Purpose .................................................................................. ii

Audience ................................................................................ ii

Contents................................................................................. ii

Prerequisites............................................................................iii

Documentation .........................................................................iii

Conventions.............................................................................iii

About T is Manual

Operation Manual: Evolution Series

Purpose

T is manual covers t e installation, routine operation, maintenance and repair of

your Evolution Dissolution Test System. It as information regarding t e

commands, menus, indicators and controls. C apter 1 provides an overview of t e

system. C apter 2 covers unpacking, installation, and qualification of t e system.

C apter 3 as operation and programming information. C apters 4 and 5 cover

maintenance and troubles ooting. Please read C apters 1, 2 and 3 before

proceeding.

Audience

T is manual is written for any person responsible for maintaining, operating or

troubles ooting t e Distek Evolution Dissolution Test System.

Contents

T is manual is divided into c apters. T e pages of t e manual are numbered

providing easy navigation to assist in finding information quickly.

T e following list describes t e material covered in eac c apter:

C apter 1 - Introduction Provides a general overview and

warnings about t e instrument.

C apter 2 - Installation Describes ow to unpack and properly

install t e unit.

C apter 3 - Operation Describes t e functionalities of t e

system and ow to run t e unit.

C apter 4 - Maintenance Explains t e steps necessary to

maintain t e unit.

C apter 5 - Troubles ooting Provides a troubles ooting c art and

description of error messages to assist

t e user if a problem arises.

Appendix A – Spare Parts and

Accessories

Provides a table of recommended and

optional spare parts.

Appendix B - Pre-Installation

Considerations: Electrical Power

Supply

Recommendation information

pertaining to electrical power supply.

Appendix C - CE Declaration of

Conformity

CE Declaration of Conformity

certificate.

Appendix D - Certificate of

Compliance

Certificate of Compliance

Appendix E - Sample Printouts from

Parallel Printer

Sample printouts for a parallel printer.

About T is Manual

Operation Manual: Evolution Series

iii

Prerequisites

T is manual assumes t at you understand t e principles of dissolution testing.

Documentation

T is manual contains important information regarding t e safe operation,

maintenance and repair of your Distek Evolution Dissolution Test System.

Conventions

T e following table contains Warnings, Cautions and Notes t at are used

t roug out t e document for your protection. Please read t is section before

using t e Evolution Dissolution Testing System.

“WARNING” statements are used in t is manual to prevent

injury to personnel.

"CAUTION: Risk of Electric Shock" statements are used to

prevent injury w en ig voltage is present.





 “CAUTION” statements are used to prevent damage to

equipment.

“NOTES” contain elpful information.

REQUIRED

ACTION

“REQUIRED ACTION” is used w ere necessary to distinguis

t e action needed from Warnings, Cautions and Notes.

Ce manuel convient aux modèles suivants

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