Distek 2500 Select Manuel utilisateur

Model 2500

Operation

Manual

Document: 3825-0001 Rev. F

Model 2500

Operation Manual

Document 3825-0001 Rev. F

121 North Center Dr. • North Brunswick, NJ 08902

Phone 732.422.7585 • Fax 732.422.7310

http://www.distekinc.com

electronic, or mechanical, including photocopying, recording, taping, or information storage and retrieval

systems - without the written permission of Distek, Inc.

Products that are referred to in this document may be either trademarks and/or registered trademarks of

the respective owners. Distek, Inc. makes no claim to these trademarks.

The information contained in the document is subject to change without notice.

While every precaution has been taken in the preparation of this document, Distek, Inc. assumes no

responsibility for errors or omissions, or for damages resulting from the use of information contained in

this document or from the use of programs and source code that may accompany it. In no event shall

Distek, Inc. be liable for any loss of profit or any other commercial damage caused or alleged to have been

caused directly or indirectly by this document.

Model 2500

DISTEK, INC.

121 North Center Drive

North Brunswick, NJ 08902

Tel. 732.422.7585

Website: http://www.distekinc.com

4Model 2500

Table of Contents

Chapter I Introduction 8

................................................................................................................................... 91 Distek Model 2500 Overview

................................................................................................................................... 112 Instrument Specification

................................................................................................................................... 123 Notices

................................................................................................................................... 144 Safety Information

................................................................................................................................... 155 Site Requirements

.......................................................................................................................................................... 16

Physical Site Consideration

.......................................................................................................................................................... 17

Electrical Requirements

................................................................................................................................... 186 Environmental Conditions

.......................................................................................................................................................... 19

Ambient Laboratory Humidity

.......................................................................................................................................................... 20

Ambient Laboratory Temperature

.......................................................................................................................................................... 21

Air Quality Considerations

.......................................................................................................................................................... 22

Environmental Considerations

Chapter II Installation 24

................................................................................................................................... 251 Unpacking

................................................................................................................................... 262 Leveling

................................................................................................................................... 273 AC Power Installation

................................................................................................................................... 284 TCS Installation

................................................................................................................................... 305 Vessel Installation

................................................................................................................................... 326 Shaft Installation

.......................................................................................................................................................... 33

Standard Shafts

.......................................................................................................................................................... 34

RTD Shafts

................................................................................................................................... 367 Paddle Installation

................................................................................................................................... 378 Basket Installation

................................................................................................................................... 389 Vessel Covers

Chapter III Installing Accessories 40

................................................................................................................................... 411 TempChek

................................................................................................................................... 422 Dosage Delivery System (DDS)

................................................................................................................................... 453 Printers

.......................................................................................................................................................... 46

Dedicated Instrument Printer

................................................................................................................................... 474 Distek Cipher Software

................................................................................................................................... 485 Agilent 8453 UV-Vis

................................................................................................................................... 496 Waters HPLC

Chapter IV Graphic User Interface (GUI) 51

................................................................................................................................... 521 2500 Dashboard

................................................................................................................................... 542 2500 RTD Dashboard

5ContentsModel 2500

................................................................................................................................... 563 2500 Select Dashboard

................................................................................................................................... 584 Apparatus ID

................................................................................................................................... 595 Methods

................................................................................................................................... 606 Reports

................................................................................................................................... 617 Settings

................................................................................................................................... 628 Logout

................................................................................................................................... 639 On-Screen Keyboard

Chapter V Operation 65

................................................................................................................................... 661 Turning On the Instrument

................................................................................................................................... 672 Operational Checkout

................................................................................................................................... 683 Height Adjustment

.......................................................................................................................................................... 69

Baskets and Paddles

.......................................................................................................................................................... 73

Modified Baskets

.......................................................................................................................................................... 75

Modified Paddles

.......................................................................................................................................................... 77

Intrinsic

................................................................................................................................... 794 Manual Run

.......................................................................................................................................................... 79

2500 with Standard Shafts

.......................................................................................................................................................... 81

2500 RTD .......................................................................................................................................................... 83

2500 Select

................................................................................................................................... 855 Create a New Method

................................................................................................................................... 886 Edit Method

................................................................................................................................... 907 Method Run

.......................................................................................................................................................... 91

Selecting a Method

.......................................................................................................................................................... 92

Using the Dosage Delivery System

.......................................................................................................................................................... 93

Simultaneous Drop Using Baskets

......................................................................................................................................................... 93

2500 with Standard Shafts

......................................................................................................................................................... 97

2500 RTD-Select

.......................................................................................................................................................... 101

Simultaneous Drop Using Paddles

......................................................................................................................................................... 101

2500 with Standard Shafts

......................................................................................................................................................... 105

2500 RTD-Select

.......................................................................................................................................................... 109

Staggered Drop Using Baskets

......................................................................................................................................................... 109

2500 with Standard Shafts

......................................................................................................................................................... 114

2500 RTD-Select

.......................................................................................................................................................... 119

Staggered Drop Using Paddles

......................................................................................................................................................... 119

2500 with Standard Shafts

......................................................................................................................................................... 124

2500 RTD-Select

................................................................................................................................... 1298 Report Summary

................................................................................................................................... 1319 User Setup

.......................................................................................................................................................... 132

New User .......................................................................................................................................................... 135

Edit User .......................................................................................................................................................... 137

Delete User

................................................................................................................................... 13810 System Settings

.......................................................................................................................................................... 139

TCS Schedule

.......................................................................................................................................................... 141

Temperature Calibration

......................................................................................................................................................... 142

Accessing Calibration

......................................................................................................................................................... 144

TCS Calibration Using TempChek

6Model 2500

......................................................................................................................................................... 146

TCS Calibration Using Reference

......................................................................................................................................................... 147

Shaft Sensor Calibration Using TempChek

......................................................................................................................................................... 150

Shaft Sensor Calibration Using Reference

.......................................................................................................................................................... 152

System Setup

......................................................................................................................................................... 156

Advanced Setup

......................................................................................................................................................... 159

LCD Calibration

.......................................................................................................................................................... 161

Service .......................................................................................................................................................... 164

Instrument Validation

.......................................................................................................................................................... 166

Battery Monitor

.......................................................................................................................................................... 168

Help

Chapter VI Maintenance 170

................................................................................................................................... 1711 General Maintenance

................................................................................................................................... 1722 Lubrication

................................................................................................................................... 1733 Belt Tension

Chapter VII Troubleshooting 175

................................................................................................................................... 1761 Prompted Messages

.......................................................................................................................................................... 177

General Messages

.......................................................................................................................................................... 180

Error Messages

.......................................................................................................................................................... 183

Warning Messages

.......................................................................................................................................................... 184

Service Messages

................................................................................................................................... 1852 LCD Display

................................................................................................................................... 1863 Power Supply

................................................................................................................................... 1874 Heating

................................................................................................................................... 1885 Stirring

................................................................................................................................... 1896 I/O Communication

................................................................................................................................... 1907 Temperature Calibration

................................................................................................................................... 1918 Mechanical

Chapter VIII Appendix A: Spare Parts and Accessories 194

Chapter IX Appendix B: Pre-Installation

Considerations 197

Chapter X Appendix C: Sample Printouts 199

Index 205

Introduction

Chapter I

IntroductionModel 2500 8

1 Introduction

Model 2500 Overview

Instrument Specification

Notices

Safety Information

Site Requirements

Environmental Conditions

This chapter contains an overview of the instrument and safeguards that need to be followed when

installing and using the instrument.

IntroductionModel 2500 9

1.1 Distek Model 2500 Overview

W elcome to a new innova tion in D issolution testing .

The Distek Model 2500 Dissolution Test System offers unmatched flexibility and configurability

while maintaining the user-friendliness that laboratories around the world have come to expect

from the preceding four generations of the 2100 series.

FEATURES

2500

2500 RTD

2500 SEL

Color Touch Screen Display

The icon driven user interface lowers overall

cost by reducing training time and user

errors while maximizing productivity and

command of the dissolution test.

YES

Electronic Qualification Guidance

Electronic qualification alerts eliminate

oversights and ensures maximum up time

and instrument availability.

YES

Quick Change Paddles and Baskets

Interchangeable stirring elements coupled

with the automatic height adjustment

provide a fast transition between Apparatus

1 and 2 without having to remove the shaft.

YES

Serialized Component Tracking

Track all serialized components including;

paddles, baskets, basket adapters, shafts

and vessels.

YES

Wireless In-Shaft Temperature Sensors

Patent Pending wireless temperature

sensors control and monitor the

temperature without the use of a wired

sensor.

YES

Patented Bathless Technology

Eliminates the water bath and all associated

maintenance while heater jackets raise

media temperatures from ambient to 37°C in

less than 15 minutes with a high

temperature capability of up to 99°C.

YES

Self-Priming Thermocirculator

The self-priming design and microprocessor

control allow for improved temperature

uniformity and heating time while the low

profile design allows the circulator to be

stowed behind the bath, requiring

no additional linear bench space.

YES

IntroductionModel 2500 10

Volume Flexibility

Accommodates up to 8 vessels ranging in

size from 100mL to 4L, allowing the user to

run a diverse range of tests.

YES

W orks w ith D istek line of D issolution equipment a nd softw are.

The instrument is compatible with the following equipment/software:

Eclipse 5300

EVO 4300 with Firmware Revision 3.01 or higher

Cipher Software

Distek Dosage Delivery System

Agilent UV-Vis 8453/8454 On-Line up to 4 baths

Waters HPLC instruments

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