Delta F DF Series Manuel utilisateur

DF Series

Oxygen Analyzer

OEM Version

Model DF-110E

Instruction Manual

Delta F Corporation

4 Constitution Way

Woburn, Massachusetts 01801-1087

Telephone: (781) 935-4600

FAX: (781) 938-0531

99000025

Rev C

031611

No part of this publication may be reproduced, stored in a retrieval system or transmitted in

any form, or by any means including electronic, mechanical, photocopying, recording or

otherwise without prior written permission of Delta F Corporation.

Stab-Eland Bi-Strataare trademarks of Delta F Corporation.

The Delta F Difference

Your Analyzer has been designed, manufactured and will be supported under

ISO-9001 controls, thus helping to insure the highest possible standards of

quality.

Every analyzer that Delta F manufactures is tested and operated on a variety of

gas concentrations to insure that it functions properly when you receive it.

The certificate of calibration assures your analyzer has been calibrated on

gases that are traceable to NIST standards. With proper maintenance, your

analyzer should remain calibrated for years.

For a fast and successful start-up, please read this manual carefully. There are

important cautions and a number of helpful hints that will help you to

optimize the operation of your analyzer.

If you have questions please do not hesitate to call the Delta F Service Line at

(781) 935-5808 or e-mail us at ser[email protected].

Table of Contents DF-110E i

1 Table of Contents

1Table of Contents ..................................................................... i

2Table of Figures ...................................................................... iv

3CAUTIONS ................................................................................ 5

3.1 Explanation of Graphic Symbols................................................................................. 5

3.2 Important Warnings .................................................................................................... 6

4Specifications .......................................................................... 7

4.1 Range .......................................................................................................................... 7

4.2 Response Time............................................................................................................ 7

4.3 Accuracy ..................................................................................................................... 7

4.4 Sample Gas Compatibility........................................................................................... 7

4.5 Sample Requirements.................................................................................................. 8

4.6 Ambient Temperature Requirements........................................................................... 8

4.7 Miscellaneous.............................................................................................................. 8

5Analyzer Start-Up Procedure .................................................. 9

5.1 Charging the Sensor .................................................................................................... 9

5.2 Powering up the Analyzer ......................................................................................... 11

5.3 Additional Capabilities.............................................................................................. 12

6Standard Features ................................................................. 13

6.1 Stable Calibration...................................................................................................... 13

6.2 Electrolyte Condition Indicator ................................................................................. 13

6.3 Analog Output........................................................................................................... 14

7Options ................................................................................... 15

7.1 Stab-El................................................................................................................... 15

7.2 Alarms....................................................................................................................... 16

7.2.1 Adjusting Oxygen Alarm Set Points ............................................................ 16

7.2.2 Alarm Relays ............................................................................................... 18

7.3 Pressure Regulators................................................................................................... 18

7.4 Filter.......................................................................................................................... 18

7.5 Low Flow Indication ................................................................................................. 18

7.6 Flow Control Valve................................................................................................... 19

7.7 Pump ......................................................................................................................... 19

7.7.1 Pump Control............................................................................................... 19

7.8 Analog Output........................................................................................................... 19

7.9 Isolated 4 to 20 mA Output ....................................................................................... 20

7.10 Gas Scale Correction Factor .................................................................................... 20

7.10.1 Adjusting the Gas Scale Factor Pot for Light Gases (He or H2) .............. 21

7.10.2 Adjusting the Gas Scale Factor Pot for Gases Heavier Than Nitrogen.... 22

8Sample Gas and Plumbing Cautions ................................... 25

8.1 Condensation............................................................................................................. 25

8.2 Temperature .............................................................................................................. 25

8.3 Leaks......................................................................................................................... 25

8.4 Process Up-sets (Oxygen Shock) .............................................................................. 26

ii DF-110E Table of Contents

9Outputs and Remote Connections........................................27

9.1 The I/O Connector .....................................................................................................27

9.1.1 Alarm 1 and 2 (NC-C-NO) ...........................................................................27

9.1.2 4 to 20 mA Isolated Output (4-20+, 4-20-)...................................................27

9.1.3 Analog Output (Rec + & Rec - )) .................................................................28

9.1.4 Remote Range Indicator (Range Com - Range 1, 2, 3) ................................28

9.1.5 Sensor Off (Sensor Off Com, Sensor Off)....................................................28

9.1.6 DC Common (DC Com)...............................................................................28

9.1.7 Ground ( )...................................................................................................29

9.1.8 Trouble Alarm ..............................................................................................29

9.2 The Remote Sensor Connector...................................................................................29

9.2.1 Remote Sensor (Sensor +, Sensor -) .............................................................29

9.2.2 Secondary Electrodes (Sec El +, Sec El -)....................................................30

9.2.3 Display Outputs (Display +, Display -) ........................................................30

9.3 Pump Control.............................................................................................................30

9.3.1 Analyzer Control of an External Pump.........................................................30

9.3.2 Remote Control of an External Pump...........................................................31

10 Maintenance and Calibration Checks...................................33

10.1 Sensor Maintenance..................................................................................................33

10.1.1 Adding Replenishment Solution...............................................................33

10.2 Calibration................................................................................................................34

10.2.1 Adjusting Calibration ...............................................................................34

10.2.2 Adjusting the Span Calibration Pot (with the GSF Option installed) .......36

11 Theory of Operation ...............................................................37

12 Troubleshooting .....................................................................39

12.1 Troubleshooting Guide.............................................................................................39

12.1.1 Problem Observations ..............................................................................39

12.1.2 Remedy Keys............................................................................................40

12.2 Troubleshooting Considerations...............................................................................41

12.2.1 Gas Pressure Effects .................................................................................41

12.2.2 Positive Pressure Operation......................................................................41

12.2.3 Negative Pressure Operation ....................................................................41

12.2.4 Temperature Effects on Sensor Performance ...........................................41

12.2.5 Replaceable Parts .....................................................................................43

12.2.6 Fuse Replacement.....................................................................................44

13 Shipping the Analyzer............................................................45

13.1 Draining the Sensor ..................................................................................................45

14 Safety and Operating Notices ...............................................47

14.1 Safety Notices...........................................................................................................47

14.2 Operating Notices.....................................................................................................47

14.3 General Warnings.....................................................................................................48

14.4 MATERIAL SAFETY DATA SHEET - Electrolyte ...............................................49

14.5 MATERIAL SAFETY DATA SHEET –Replenishment Solution ..........................55

14.6 Seguridad..................................................................................................................58

14.7 Avisos Generales......................................................................................................59

14.8 Sicherheitshinweis....................................................................................................60

14.9 Allgemeine Warnhinweise........................................................................................61

14.10 Mesures de sécurité ..............................................................................................62

14.11 Precautions à prendre en general..........................................................................63

14.12 Misure di sicurezza...............................................................................................64

14.13 Precauzioni da prendere in generale:....................................................................65

Table of Contents DF-110E iii

15 Warranty ................................................................................. 67

16 Index ....................................................................................... 69

iv DF-110E Table of Figures

2 Table of Figures

Figure 1: Delta F Oxygen Sensor...................................................................... 9

Figure 2: Sensor Off Switch............................................................................ 11

Figure 3: Power Switch................................................................................... 11

Figure 4: Electrolyte Condition Indicator ....................................................... 13

Figure 5: Setting alarms .................................................................................. 16

Figure 6: Gas Correction Factor Adjustment.................................................. 22

Figure 7: I/O Connector Pin-out ..................................................................... 27

Figure 8: Remote Sensor Connector Pin-out .................................................. 29

Figure 9: Calibration Controls ........................................................................ 35

Figure 10: Span Adjust with GSF installed .................................................... 36

Figure 11: Sensor Layout ................................................................................ 37

CAUTIONS DF-110E 5

3 CAUTIONS

There are a number of warnings and cautions that must be observed to avoid

damage to the analyzer as well as insuring the safety of its users. The analyzer

must be operated in a manner specified in this manual. Delta F cannot be

responsible for direct or consequential damages that result from installing

and/or operating the analyzer in a manner not described in this manual.

Importantly, the analyzer has been designed for use with inert, non-toxic, non-

combustible sample gasses only. Delta F cannot be responsible for direct or

consequential damages that result from using the analyzer with these gases.

3.1 Explanation of Graphic Symbols

Following is a list of the various symbols used throughout this manual and

their definitions.

CAUTION

This symbol alerts the user to the presence of physically

hazardous conditions that may be dangerous to individuals or

equipment.

NOTE

This symbol alerts the user to the presence of important

operations and/or maintenance information.

This symbol alerts the user to the presence of caustic liquid.

Refer to the MSDS at the back of the manual for handling

instructions.

6DF-110E CAUTIONS

3.2 Important Warnings

DANGER

Potentially hazardous AC voltages are present within this instrument.

Leave all servicing to qualified personnel. Disconnect the AC power

source when installing or removing: external connections, the sensor,

the electronics, or when charging or draining electrolyte.

CAUTION

Do not operate this Oxygen Analyzer without a complete

understanding of the instructions in this manual. Do not connect this

Analyzer to a power source until all signal and plumbing

connections are made.

CAUTION

This analyzer must be operated in a manner consistent with its

intended use and as specified in this manual.

Specifications DF-110E 7

4 Specifications

4.1 Range

DF-110 Single Range Analyzer

Range (ppm)

DF-110

Model #

Range (%)

DF-110

Model #

0 to 5,000 ppm

111-5000

0 to 25%

111-P25

0 to 1,000 ppm

111-1000

0 to 10%

111-P10

0 to 500 ppm

111-500

0 to 5%

111-P5

0 to 100 ppm

111-100

0 to 1%

111-P1

0 to 50 ppm

111-50

0 to 10 ppm

111-10

DF-110 Three Range Analyzer

Ranges (ppm)

DF-110

Model #

Ranges (%)

DF-110

Model #

0 to100/1,000/10,000 ppm

113-10000

0 to 0.25/2.5/25%

113-P25

0 to 50/500/5,000 ppm

113-5000

0 to 0.1/1/10%

113-P10

0 to 10/100/1,000 ppm

113-1000

0 to 0.05/0.5/5%

113-P5

0 to 5/50/500 ppm

113-500

0 to 1/10/100 ppm

113-100

4.2 Response Time

Responds instantaneously to O2change. Equilibrium time depends on specific

conditions. Typically less than 10 seconds to read 90% of a step change.

4.3 Accuracy

At constant conditions, the greater of +/- 3% or 0.5% of measurement range,

but not lower than 0.05% of full analyzer range for three range analyzers.

4.4 Sample Gas Compatibility

Standard Sensor

All inert and passive gases including N2, H2, CO, freons, light hydrocarbons,

etc.

8DF-110E Specifications

Sensor with Stab-El

Neutralizes contaminants including acids such as CO2, H2S, Cl2, NOX, SOX,

etc. (See page 15 for concentration limits).

4.5 Sample Requirements

Gas phase, non-condensing, sample temperature: -17 to 45°C (0 to 113°F).

Flow rate 1.0 to 2.0 scfh at 0.2 to 1.0 psig pressure.

4.6 Ambient Temperature Requirements

Room/cabinet temperature: 0 to 45°C (32 to 113°F)

4.7 Miscellaneous

Store and operate between 0°C and 45°C (32°F and 113°F).

100-120/200-240 VAC, 50-60 Hz, 1.0/0.5 A maximum

Nominal power consumption 20 Watts

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