Agilent Technologies 8000 Series Manuel utilisateur

Agilent Technologies

Agilent 8000

Dissolution Sampling

Station

Operator’s Manual

8000 Operator’s Manual

Notices

No part of this manual may be reproduced

in any form or by any means (including

electronic storage and retrieval or transla-

tion into a foreign language) without prior

agreement and written consent from Agi-

lent Technologies, Inc. as governed by

United States and international copyright

laws.

Manual Part Number

70-9060

Edition

Rev C, May 2014

Agilent Technologies, Inc.

3501 Stevens Creek Blvd.

Santa Clara, CA 95052 USA

Warranty

The material contained in this doc-

ument is provided “as is,” and is

subject to being changed, without

notice, in future editions. Further,

to the maximum extent permitted

by applicable law, Agilent disclaims

all warranties, either express or

implied, with regard to this manual

and any information contained

herein, including but not limited to

the implied warranties of mer-

chantability and fitness for a par-

ticular purpose. Agilent shall not be

liable for errors or for incidental or

consequential damages in connec-

tion with the furnishing, use, or

performance of this document or of

any information contained herein.

Should Agilent and the user have a

separate written agreement with

warranty terms covering the mate-

rial in this document that conflict

with these terms, the warranty

terms in the separate agreement

shall control.

Technology Licenses

The hardware and/or software described in

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license and may be used or copied only in

accordance with the terms of such license.

Restricted Rights Legend

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rights customarily provided to end user

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cal Data - Commercial Items) and DFARS

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puter Software or Computer Software

Documentation).

Safety Notices

CAUTION

A CAUTION notice denotes a

hazard. It calls attention to an

operating procedure, practice, or

the like that, if not correctly per-

formed or adhered to, could result

in damage to the product or loss

of important data. Do not proceed

beyond a CAUTION notice until

the indicated conditions are fully

understood and met.

WARNING

A WARNING notice denotes a

hazard. It calls attention to an

operating procedure, practice,

or the like that, if not correctly

performed or adhered to, could

result in personal injury or

death. Do not proceed beyond a

WARNING notice until the

indicated conditions are fully

understood and met.

8000 Operator’s Manual 3

Contents

Figures 7

Tab les 9

1Safety 11

Electrical Hazards 12

Warning 13

Caution 13

Note 13

Information Symbols 14

2 Introduction 15

8000 with Peristaltic Pump 17

Conventions Used in this Manual 17

Serial Number Format 18

3 Setting Up the 8000 19

Unpacking of 8000 and Components 20

Unpacking Your 8000 21

Unpacking / Setup of 8000 & Peristaltic Pump 22

Unpacking / Setup of 8000 & Syringe Pump 26

Unpacking / Setup of 8000, Syringe Pump, and Filter

Changer 29

Setup of 8000 and Components 34

Installing 8000 Full Flow Filters 34

Power and Network Connections 34

Installing the Sample Tray 36

48000 Operator’s Manual

Contents

Installing the Media Rinse Reservoir 36

Installing and Connecting the Autocalibration Block

(Peristaltic Pump only) 37

Installing the RM Module 38

Loading Filters (Filter Changer only) 40

Changing Filter Types (Filter Changer Only) 40

Hidden Key Functions 41

4 Operating the 8000 45

Operating the 8000 with Apparatus 1 / 2 46

8000 Keypad Options 46

8000 Menu Options - Apparatus 1 / 2 48

Creating a Sample Program 61

Starting a 8000 Program 66

Operating the 8000 with Apparatus 3 / 7 72

8000 Keypad Options 72

8000 with Apparatus 3 / 7 - Menu Options 74

Creating a Sample Program 86

Starting a Program 91

Manual Sample 95

Volumetric Calibration (Peristaltic Pump only) 97

Automatic Calibration 97

Manual Calibration 99

Checking the Calibration - Volume Accuracy 101

Daisy Chaining 102

Printer Operation and Communications 103

5 Maintenance and Troubleshooting 105

Preventive Maintenance 106

Clean System with Peristaltic Pump 106

Clean System Function with Syringe Pump 111

Contents

8000 Operator’s Manual 5

Syringe and Seal Replacement 112

Cleaning the Syringes 113

System Cleaning Procedure with Syringe Pump and Filter

Changer (optional) 115

Cleaning the Filter Changer Drip Tray 117

Cleaning the Media Replacement Pump 117

Report Center Impact Printer 119

Installing the Cartridge Ribbon 119

Replacing a Paper Roll 120

Toggling Your Printer Online 121

Printer Self Test 121

Printer Configuration 122

Obtaining Warranty and Other Services 123

Index 125

68000 Operator’s Manual

Contents

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8000 Operator’s Manual 7

Figures

Figure 1. Agilent 8000 Dissolution Sampling Station 21

Figure 2. Peristaltic Pump 22

Figure 3. Cable Connections for 8000, Peristaltic Pump, and VK

7000 / 7010 24

Figure 4. Resident Probe 25

Figure 5. 806 Syringe Pump 26

Figure 6. Cable Connections for 8000, Syringe Pump, and VK

7000 / 7010 27

Figure 7. Y Cable 5075-0446 and Adapter 5075-0852 28

Figure 8. 808 Filter Changer 30

Figure 9. Cable Connections for 8000, Syringe Pump, Filter

Changer, and VK 7000 / 7010 31

Figure 10. Y Cable 5075-0446 and Adapter 5075-0852 32

Figure 11. Resident Probe Housing and Sample Cannula 33

Figure 12. Internal Media Replacement Module 38

Figure 13. External Media Replacement Module 39

Figure 14. 8000 Keypad 46

Figure 15. 8000 Keypad 72

Figure 16. The Cleaning Process 108

88000 Operator’s Manual

Figures

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8000 Operator’s Manual 9

Tables

Table 1. Hidden Key Functions 41

Table 2. Front Panel Options (Apparatus 1 / 2) 47

Table 3. Main Menu Options (Apparatus 1 / 2) 49

Table 4. Set Clock and Alarms Options (Apparatus 1 / 2) 51

Table 5. Disso Parameters Options (Apparatus 1 / 2) 53

Table 6. Set Syringe Pump Parameters (Apparatus 1 / 2) 55

Table 7. Disso Control/Monitor Options (Apparatus 1 / 2) 57

Table 8. Manual Operations Options (Apparatus 1 / 2) 58

Table 9. Operate Syringe/Filter Changer Options (Apparatus 1 /

2) 59

Table 10. Program Variables Options (Apparatus 1 / 2) 62

Table 11. Select Start Mode Options (Apparatus 1 / 2) 68

Table 12. Disso Options (Apparatus 1 / 2) 69

Table 13. Select Disso Program Start Mode Options (Apparatus

1 / 2) 71

Table 14. Front Panel Options (Apparatus 3 / 7) 73

Table 15. Main Menu Options (Apparatus 3 / 7) 75

Table 16. Set Clock and Alarms Options 77

Table 17. Set App 3/7 Parameters Options (Apparatus 3 /

7) 79

Table 18. Set Syringe Pump Parameters Options (Apparatus 3 /

7) 81

Table 19. App 3/7 Control/Monitor Options 83

Table 20. Manual Operations (Apparatus 3 / 7) 84

Table 21. Operate Syringe/Filter Changer Options 85

Table 22. Program Variables Options (Apparatus 3 / 7) 88

Table 23. Select Start Mode Options (Apparatus 3 / 7) 93

Table 24. App 3/7 Options 94

10 8000 Operator’s Manual

Tables

Table 25. Manual Sampling Options 95

Table 26. Volume Accuracy Parameter Options 101

Table 27. Print Selections Options 104

Table 28. Program Auto Clean Variables 110

Table 29. Disso Parameters. 115

Table 30. Program Variables 116

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