Agilent Technologies 1260 Infinity Manuel utilisateur
Agilent Technologies
Agilent 1260 Infinity
Standard Autosampler
User Manual
Agilent 1260 Infinity Standard Autosampler User Manual
Notices
© Agilent Technologies, Inc. 2007-2012,
2013
No part of this manual may be reproduced
in any form or by any means (including elec-
tronic storage and retrieval or translation
into a foreign language) without prior agree-
ment and written consent from Agilent
Technologies, Inc. as governed by United
States and international copyright laws.
Manual Part Number
G1329-90015 Rev. B
Edition
04/2013
Printed in Germany
Agilent Technologies
Hewlett-Packard-Strasse 8
76337 Waldbronn
This product may be used as a com-
ponent of an in vitro diagnostic sys-
tem if the system is registered with
the appropriate authorities and com-
plies with the relevant regulations.
Otherwise, it is intended only for gen-
eral laboratory use.
Warranty
The material contained in this docu-
ment is provided “as is,” and is sub-
ject to being changed, without notice,
in future editions. Further, to the max-
imum extent permitted by applicable
law, Agilent disclaims all warranties,
either express or implied, with regard
to this manual and any information
contained herein, including but not
limited to the implied warranties of
merchantability and fitness for a par-
ticular purpose. Agilent shall not be
liable for errors or for incidental or
consequential damages in connection
with the furnishing, use, or perfor-
mance of this document or of any
information contained herein. Should
Agilent and the user have a separate
written agreement with warranty
terms covering the material in this
document that conflict with these
terms, the warranty terms in the sep-
arate agreement shall control.
Technology Licenses
The hardware and/or software described in
this document are furnished under a license
and may be used or copied only in accor-
dance with the terms of such license.
Restricted Rights Legend
If software is for use in the performance of a
U.S. Government prime contract or subcon-
tract, Software is delivered and licensed as
“Commercial computer software” as
defined in DFAR 252.227-7014 (June 1995),
or as a “commercial item” as defined in FAR
2.101(a) or as “Restricted computer soft-
ware” as defined in FAR 52.227-19 (June
1987) or any equivalent agency regulation
or contract clause. Use, duplication or dis-
closure of Software is subject to Agilent
Technologies’ standard commercial license
terms, and non-DOD Departments and
Agencies of the U.S. Government will
receive no greater than Restricted Rights as
defined in FAR 52.227-19(c)(1-2) (June
1987). U.S. Government users will receive
no greater than Limited Rights as defined in
FAR 52.227-14 (June 1987) or DFAR
252.227-7015 (b)(2) (November 1995), as
applicable in any technical data.
Safety Notices
CAUTION
A CAUTION notice denotes a
hazard. It calls attention to an
operating procedure, practice, or
the like that, if not correctly per-
formed or adhered to, could
result in damage to the product
or loss of important data. Do not
proceed beyond a CAUTION
notice until the indicated condi-
tions are fully understood and
met.
WARNING
A WARNING notice denotes a
hazard. It calls attention to an
operating procedure, practice,
or the like that, if not correctly
performed or adhered to, could
result in personal injury or
death. Do not proceed beyond a
WARNING notice until the indi-
cated conditions are fully under-
stood and met.
Agilent 1260 Infinity Standard Autosampler User Manual 3
In This Book
In This Book
This manual covers the Agilent 1260 Infinity Standard Autosampler (G1329B).
1 Introduction to the Autosampler (ALS)
This chapter gives an introduction to the autosampler and instrument
overview.
2 Site Requirements and Specifications
This chapter provides information on environmental requirements, physical
and performance specifications.
3 Installing the Autosampler
This chapter provides information on unpacking, checking on completeness,
stack considerations and installation of the module.
4 Using the Autosampler
This chapter provides information on how to set up the module for an analysis
and explains the basic settings.
5 Optimizing Performance
This chapter provides information on how to optimize the module.
6 Troubleshooting and Diagnostics
Overview about the troubleshooting and diagnostic features.
7 Error Information
This chapter describes the meaning of error messages, and provides
information on probable causes and suggested actions how to recover from
error conditions.
4 Agilent 1260 Infinity Standard Autosampler User Manual
In This Book
8 Maintenance
This chapter describes the maintenance of the module.
9 Parts and Materials for Maintenance
This chapter provides information on parts for maintenance.
10 Identifying Cables
This chapter provides information on cables used with the module.
11 Hardware Information
This chapter describes the detector in more detail on hardware and
electronics.
12 Appendix
This chapter provides addition information on safety, legal and web.
Agilent 1260 Infinity Standard Autosampler User Manual 5
Contents
Contents
1 Introduction to the Autosampler (ALS) 9
Introduction to the Autosampler (ALS) 10
2 Site Requirements and Specifications 21
Site Requirements 22
Physical Specifications 25
Performance Specifications Standard Autosampler 26
3 Installing the Autosampler 27
Unpacking the Autosampler 28
Optimizing the Stack Configuration 29
Installing the Autosampler 32
Flow Connections 35
Installing the Sample Tray 37
Transporting the Autosampler 38
4 Using the Autosampler 39
Sample Trays 40
Choice of Vials and Caps 42
5 Optimizing Performance 45
Optimization for Lowest Carry-over 46
Fast Injection Cycle and Low Delay Volume 49
Precise Injection Volume 51
Choice of Rotor Seal 53
6 Troubleshooting and Diagnostics 55
Overview of the Module’s Indicators and Test Functions 56
Status Indicators 57
Maintenance Functions 59
ALS Step Commands 66
6 Agilent 1260 Infinity Standard Autosampler User Manual
Contents
Troubleshooting 68
Troubleshooting Guide for the Sample Transport Assembly 70
Agilent Lab Advisor Software 77
7 Error Information 79
What are Error Messages 81
General Error Messages 82
Autosampler Error Messages 88
8 Maintenance 101
Introduction to Maintenance 102
Cautions and Warnings 103
Updating the Firmware 105
Cleaning the Module 106
Safety Flap, Flex Board 107
Transport Assembly Parts 108
Maintenance Functions 109
Simple Repairs 110
Exchanging the Needle Assembly 111
Exchanging the Needle-Seat Assembly 114
Exchanging the Rotor Seal 116
Exchanging the Metering Seal and Piston 120
Exchanging the Gripper Arm 124
Exchanging the Interface Board 126
Replacing the Module’s Firmware 127
9 Parts and Materials for Maintenance 129
Main Assemblies 130
Analytical-Head Assembly 132
Vial Trays 134
Standard Autosampler Accessory Kit 136
Maintenance Kit 137
Injection Upgrade Kit 138
Multi-Draw Kit 139
External Tray 140
Agilent 1260 Infinity Standard Autosampler User Manual 7
Contents
10 Identifying Cables 141
Cable Overview 142
Analog Cables 144
Remote Cables 146
BCD Cables 149
External Contact Cable 151
CAN/LAN Cables 152
Auxiliary Cable 153
RS-232 Cables 154
11 Hardware Information 155
Firmware Description 156
Interfaces 159
Setting the 8-bit Configuration Switch 166
Electrical Connections 170
Early Maintenance Feedback (EMF) 172
Instrument Layout 173
12 Appendix 175
General Safety Information 176
The Waste Electrical and Electronic Equipment (WEEE) Directive
(2002/96/EC) 179
Lithium Batteries Information 180
Radio Interference 181
Solvent Information 182
Sound Emission 184
Agilent Technologies on Internet 185
8 Agilent 1260 Infinity Standard Autosampler User Manual
Contents
9
Agilent 1260 Infinity Standard Autosampler User Manual
Agilent Technologies
1
Introduction to the Autosampler (ALS)
Introduction to the Autosampler (ALS) 10
Sampling Sequence 12
Sampling Unit 15
Transport Assembly 18
This chapter gives an introduction to the autosampler and instrument overview.
10 Agilent 1260 Infinity Standard Autosampler User Manual
1Introduction to the Autosampler (ALS)
Introduction to the Autosampler (ALS)
Introduction to the Autosampler (ALS)
Figure 1 Overview of the Autosampler
The Agilent 1260 Infinity autosampler is designed for use with other modules
of the Agilent 1200 Infinity Series, 1200 Series and 1100 Series LC, or with
other LC systems if adequate remote control inputs and outputs are available.
The autosamplers are controlled by the Agilent Instant Pilot (G4208A) or by
Agilent control software (OpenLAB CDS, ChemStation for LC, EZChrom Elite
etc.).
Three sample-rack sizes are available for the autosampler. The standard
full-size rack holds 100 × 1.8 mL vials, while the two half-size racks provide
space for 40 × 1.8 mL vials and 15 × 6 mL vials respectively. Any two half-size
rack trays can be installed in the autosampler simultaneously. A specially
designed sample-rack holding 100 × 1.8 mL vials is available for use with
thermostatted autosamplers. The half-size racks trays are not designed for an
optimal heat transfer when they are used with a thermostatted autosampler.
6cVani^XVa]ZVY
<g^eeZgVgb
CZZYaZhZVi
K^VaigVn
Hl^iX]^c\kVakZ
Autres manuels pour 1260 Infinity
19
Table des matières
Autres manuels Agilent Technologies Équipement de laboratoire
Agilent Technologies
Agilent Technologies N1021B Manuel utilisateur
Agilent Technologies
Agilent Technologies 2200 TapeStation Manuel utilisateur
Agilent Technologies
Agilent Technologies 850-DS Manuel utilisateur
Agilent Technologies
Agilent Technologies 7200 Manuel d'utilisation
Agilent Technologies
Agilent Technologies 1260 Infinity Manuel utilisateur
Agilent Technologies
Agilent Technologies Magnis NGS Prep System Manuel utilisateur
Agilent Technologies
Agilent Technologies Intuvo 900 Guide de l'utilisateur
Agilent Technologies
Agilent Technologies InfinityLab LC Series Manuel utilisateur
Agilent Technologies
Agilent Technologies 1290 infinity Manuel utilisateur
Agilent Technologies
Agilent Technologies 1260 Infinity II Quaternary System Manuel utilisateur
Agilent Technologies
Agilent Technologies 8494G Manuel de service
Agilent Technologies
Agilent Technologies 4107 Manuel utilisateur
Agilent Technologies
Agilent Technologies InfinityLab LC Series Manuel utilisateur
Agilent Technologies
Agilent Technologies 7890 Series Mode d'emploi
Agilent Technologies
Agilent Technologies 11970 Series Manuel utilisateur
Agilent Technologies
Agilent Technologies Archon Mode d’emploi
Agilent Technologies
Agilent Technologies 7694 Manuel utilisateur
Agilent Technologies
Agilent Technologies 2200 TapeStation Manuel utilisateur
Agilent Technologies
Agilent Technologies G1701EA Manuel utilisateur
Agilent Technologies
Agilent Technologies 7000 Triple Quadrupole GC/MS Manuel utilisateur
Agilent Technologies
Agilent Technologies HS-16 Manuel utilisateur
Agilent Technologies
Agilent Technologies CrossLab RapidFire 400 Manuel utilisateur
Agilent Technologies
Agilent Technologies TriScroll Exhaust Silencer Kit Manuel utilisateur
Agilent Technologies
Agilent Technologies 7820A Manuel utilisateur
